动物胶凝聚重量法测定含金石英石中二氧化硅.pdfVIP

.57 . 何 梅:动物肢凝聚重量法测定含金石英石中二氧化硅 第 5 期 动物胶凝聚重量法测定含金石英石中二氧化硅 何梅 (大冶有色设计研究院有限公司分析测试中心，湖北黄石 435:∞5) 摘要:采用氢氧化制熔融试样，水提取，加盐酸蒸于后盐酸介质中加动物胶凝聚，过滤分离杂质元素盐类，沉淀灼烧后称重，滤液中 可溶性二氧化硅采用电感搞合等离子体原子发射光谱法测定。按照实验方法测定含金石英石实际样品，结果的相对标准偏差 (RSD ,n =7) 为 0.11%-0.17% ，测定值与国标法的测定结果基本吻合。 关键词:熔融;提取;动物胶凝聚;灼烧:电感偶合等离子体原子发射光谱法测定 文章编号:1 ∞8 -021X(2016)05- ∞57 -02 中图分类号:0657.31 文献标tR码:A Determination of Silicon Dioxide in Gold Bearing Quartz by the Method of Agglomeration Weight of Animal Glue He Mei ( Analysis and Testing Center , Dayie Non - ferrous Melals D自ign and Research Institute Co. , Ltd. ,Huangshi 435∞15 ,China) Abstract: Using sodium hydroxide mo1ten specimen , water extraction , and evaporation 10 dryness of the hydrochloric acid and hydrochlOric acid medium with gelatin coagulatiOn ,filtratiOn and separation imp旧ity element salts ,ignition of precipita忧 after weighing , sOluble silica in the filtrate by induclively coupled plasma atomic emission spec甘ometry for the delermination. According 10 experimenlal melhod for determination of the conlenl of stOne inscriptions of actual samples ，由e relative standard deviation (RSD ,n = 7) ranged frOm O. 11% tO O. 17%. DeterminatiOn Of values and national standard method of determinaliOn results a陀 hasically cOnsistent. Key words: melting ó extractiOn ó animal glue cOndensatiOn ó bum; determination by inductively coupled plasma atomic emlsSlon spectrometry 要求。本文采用电感搞合等离子体原子发射光谱法对滤液 含金石英石是铜冶炼过程中必不可少的熔剂之一，炉中