4卷(外国英语资料).docVIP

4卷 First, fill in the blanks (1 points per minute, 20 points) 1, if you maintain the original degree of heating, no longer distilled liquid evaporation, the temperature suddenly dropped, you should (), even if the quality of very few can not be steamed dry. 2, () is separated and purified with water immiscible volatile organic compounds commonly used methods. 3. In a vacuum distillation unit, the sodium hydroxide column is mainly used for absorption (and water). 4, the capillary method to determine the melting point, usually with the capillary inside diameter (), filling the sample height is (). If the sample is not refined and the packing is not tight, the melting point is determined. 5, the boiling point of matter varies with the atmospheric pressure, usually referred to as boiling point. 6. The volume of the separating funnel is at least greater than the volume of the liquid being divided. Separate the mixture with a separate funnel; the upper layer is from () and from the lower layer. 7, from the fat extractor () () and () is the use of the solid, continuous pure solvent extraction, this device has high efficiency, saving reagent, but the material is not easy to use (). 8, the crude product of n-butyl bromide after washing oil that contains a reddish brown, (). Can be removed with a small amount (of). 9, the direct esterification catalyzed by acid is the most important method for preparing carboxyl esters in laboratory, and the commonly used catalysts are (,), () and () and so on. 10., in order to avoid crystallization in the funnel during heat filtration, the funnel can be used. Two, multiple-choice questions. (2 points per game, 20 points) 1, the long aniline is reddish brown, refined by () method. A, filtration, B, activated carbon decolorization C, distillation, D, steam distillation 2. The amount of distillation at a certain pressure should be estimated before vacuum distillation. A, boiling point B, shape C, melting point, D, solubility 3, in the process