管式个体采样器测定空气中甲醛的研究.pdfVIP

中国卫生检验杂志2007年12月第l7卷第12期 Chinese Journal of Health Laboratory Technology，Dec 2007；Vol 17 No 12 2229 【化学测定方法】 管式个体采样器测定空气中甲醛的研究 尹洪银 ，邵华h，高希宝 ，张春玲 (1．山东省职业卫生与职业病防治研究院，济南 250062；2．山东大学公共卫生学院，济南 250012) [摘要] 目的：研制测定空气中甲醛的被动式个体采样器。方法：根据费克第一扩散定律设计新型被动式个体采样器， 并对采样器的性能指标进行评价。结果：在温度10(℃～40(℃，湿度20％一40％，风速50—600 cm／s的范围内，被动式采 样器测定空气中甲醛采样流量：104．05 ml／min，最大吸附容量0．2751 mg，最短采样时间为30 min，用前稳定性t30 d，样 品稳定性≥14 d，精密度RSD为5．34％。结论：研制的个体采样器可以作为一种测定空气中甲醛的新型采样仪器。 [关键词] 被动式；甲醛；个体采样器 [中图分类号] R134 ．4 [文献标识码] A [文章编号] 1004—8685(2007)12—2229—03 Tube—type passive personal sampler for determination of formaldehyde in air Y／nHong-y~’，-，ShaoHua ，C,aoXi-bao ，Zhang(；hun-linf (1．Shandong Academy of Occupational and Occupational Medicine，Jinan 250062，China；2．School of Public Health，Shandong University，Jinan 250012，China) [Abstract] 0bjective：To design a passive personal sampler for the determination of the formaldehyde in the air．Methods：A new passive personal sam pler Was designed based on t}le Fick first law of diflusion and its function Was evaluated in the laboratory．Results：Under the condition of wind velocity of 50～60o cm／s，relative humidity of 20％ 一40％ and temperature of IO~C一40℃，the sampling rate of the passive sampler Was 104．5 ml／min，the capacity Was 0．275 1 mg，the shortest sampling time Was 30 min，the shelf life was more than 30 d，the storage stability Was more t}lan 14 d and the precision Was 5．34％．Condu- sion：rI’}lis new kind of passive personal sam pler Can be used as a new device for the determination of the formaldehyde in the air． [Key words] Passive；Formaldehyde；Personal sampler 随着经济的发展，人民对生活水平的要求提高，各种装修 1 材料与方法 材料及高级家具逐渐步入越来越多的家庭，但装饰材料中有 1．1 仪器和试剂 毒有害物质的含量没有得到有效控制，随之而来的环境问题，