如何用真空蒸发结晶法制取无水硫酸钠的方法（How to use vacuum evaporation crystallization method to remove sodium sulfate）.doc

如何用真空蒸发结晶法制取无水硫酸钠的方法（How to use vacuum evaporation crystallization method to remove sodium sulfate） How to remove sodium sulphate from vacuum evaporation crystallization method. TXT love is a strong word. The upper half of it is derived from metamorphosis and the lower half is derived from abnormal state. Sodium sulfite is used in vacuum evaporation crystallization method Li shuping, liu youzhi (chemical engineering department of north China institute of technology, taiyuan 030051, shanxi) Anhydrous sodium sulfate and sodium sulphate, which are widely used in the production of sodium sulfide, sodium silicate, ultramarine blue, etc . Can also be used in the manufacture of glass, paper making, washing agent, soap, dyes, synthetic fiber, leather, medicine and ceramic industries, is a kind of important chemical raw materials [1]. 1 experimental principle The commonly used method to produce anhydrous sodium sulfate have mirabilite encapsulation-dehydration, reforming process, by-product encapsulation-dehydration method, calcium mirabilite method 1 mirabilite is divided into soluble evaporation encapsulation-dehydration evaporation and encapsulation-dehydration, hot melt, hot melt salting-out encapsulation-dehydration [2]. The authors adopt vacuum water ring vacuum pump, with D TB (diversion tube - plate) crystallizer with vacuum evaporation crystallization directly from the industrial crude glaubers salt crystallization of anhydrous sodium sulfur acid this method has short process, less equipment, small investment, product granularity, purity, easy control, etc. According to the material balance figure [1] (see figure 1), can determine in what form the substance of crystallization from solution. Can be seen from the curve in figure 1, the solubility of sodium sulfate curve has three inflection point A, B, C, including the temperature of the point B is 32. 4 ℃. When T 32. 4 ℃, the solubility of sodium sulfate in aqueous solution with the increase of the temperature incre