烟用香精的极性偶合柱系统分析 - 食品与生物技术学报.PDF

第29 卷第2 期 食 品 与生 物 技 术学 报 Vol. 29 No.2 2010 年3月 Journal of Food Scienceand Biotechnology Mar. 2010 : 1673-1689( 2010)02-0215-04 烟用香精的极性偶合柱系统分析 熊国玺, 王娜, 司辉, 朱巍, 熊 斌, 李 丹 (湖北中烟工业公司技术中心,湖北武汉430040) : 为提高烟用香精分析结 的可靠性,针对在单柱气相色谱/质谱(GC/MS) 上分离峰效 不佳或色谱图中有明显重叠峰的烟用香精, 作者采用极性偶合柱系统GC/MS 进行了定性分析, 并 优化分析条件,与单柱GC/ MS 分析结 进行比较最后,比较了不同分析结 所得化学成分和品 吸结 之间的对应关系结 表明,极性偶合柱系统GC/MS 比单柱 GC/MS 具有更强的分离能 力,可定性的组分明显多于一维GC/ MS,并且更符合该香精的评吸结 这种分析方法有利于更 全面地认识香精的化学成分, 更准确地认识香精的组成与功能之间的关系为增强加香配方研究 的科学性提高调香工作的效率提供有力的支持 : 烟用香精; 定性分析;极性偶合柱系统 : TS 411 : A Development of aPolar Coupling Column System to Analysis Tobacco Flavors XIONG Guo-xi, WANG Na, SI Hui, ZHU Wei, XIONG Bin, LI Dan (T echnology Center of China Tobacco Hubei Industrial Corporation, Wuhan 430040, China) Abstract:The aim of this study is to increase accuracy of tobacco flavors analysis results, for this, a polar coupling column system was adopted to optimize, analysize and comprise with GC/MS analysis results and the relationship between taste and chemical compounds obtained by different analysis resultswas comprised. The results showed that polar coupling column system exhibited greater separate ability, the compounds qualified were much more than that of one-dimensional GC/MS and has higher accordance to the taste result. Those results has proven that the system can fully qualify chemical compounds in tobacco flavors and , increase scientific nature and efficiency of flavor blending. Key ords: tobacco flavor, quality analysis, polar coupling column system GC//MS , ,( GC) , ,