原创力文档Annealing dependence of the superconductivity of Pb0.65Sr2.35Y0.5Ca0.5Cu2Oy：（退火Pb0.65Sr2.35Y0.5Ca0.5Cu2Oy的超导的依赖）.pdfVIP
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Annealing dependence of the superconductivity of
Pb Sr Y Ca Cu O
0.65 2.35 0.5 0.5 2 y
H. JIN , K. Q. RUAN , L. B. WANG, Y. M. QIU , C. Y. WANG , Y. Q. ZHOU ,
X. D. CUI , L. Z. CAO , Z. J. CHEN , Y. H. ZHANG
Structure Research Laboratory and Department of Physics, University of Science and
Technology of China, Hefei, Anhui 230026, People’s Republic of China
L. ZHOU
Physics Department, Anhui Normal University, Wuhu, Anhui 241000, People’s Republic of
China
The effect of annealing conditions on the superconductivity of the Pb-based 1 2 1 2 phase
Pb Sr Y Ca Cu O system was studied. The weight change of the samples was
0.65 2.35 0.5 0.5 2 y
measured by thermogravimetric analysis (TGA). The phases occurring in the samples were
detected by X-ray diffraction (XRD) and their superconducting transitions were determined
by alternating current (a.c.) susceptibility measurements. The results showed that the
oxygen occupancy sites of the samples annealed under various conditions were different,
and the oxygen content or oxygen occupancy site affected the phase formation of the
sample. It has been found that there is an optimum value of oxygen content at which T is the
highest, and the highest T can be obtained only within a very narrow range of oxygen
content.
1. Introduction
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