原创力文档Application of a mathematical model to the study of the glass transition temperature in polymer electrolyte precursor systems：（应用数学模型研究玻璃化转变温度的聚合物电解质前驱系统）.pdfVIP
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Polymer Bulletin 38, 353-357 (1997) Polymer Bulletin
9 Springer-Verlag 1997
Application of a mathematical model to the study
of the glass transition temperature in polymer electrolyte
precursor systems
C. del Rio 1,P. J. Martin-Alvarez 2, J. L. Acosta 1
i Instituto de Ciencia y Tecnologia de Polimeros (C.S.I.C.)
2 Instituto de Fermentaciones tndustriales (C.S.I.C.), Juan de la Cierva, 3,
E-28006 Madrid, Spain
Received: 18November 1996/Revisedversion: 2 December 1996/Accepted:3 December 1996
Abstract
To the purpose of studying the effect of composition on the glass transition temperature (Tg)
of a series of polymer electrolytes based on blends of polyethylene oxide (PEO), poly
(octafluoropentoxytrifiuoroethoxy)pliosphazene (PPz) and poly(epichlorhydrine), a
mathematical model was applied to results obtained through DSC determination using seven
ternary blends selected by an experimental design. The parameters of the model were chosen
by means of stepwise linear regression method. The final model proved to be appropriate
(Rz=-0.997; s=0.99 K) to predict the Tg values. From a structural point of view it was found
that the lowest Tg values were obtained for the blends containing the smallest PECH portion.
Introduction
The use of polymeric electrolytes in advanced rechargeable solid state batteries has gained
considerable scientific and technological interest, due to the fact that these devices may, in the
near future, constitute an alternate energy source to the conventional petrochemical sources
of today, thus combining attractive economic perspectives with environmental benefits (1-4).
Our research group has been developing since some time new polymer electrolytes based on
polyether blends (PEO, PECH) and polyphosphazenes (PPz) with the ai
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