原创力文档Application of EPMA to the localization and speciation of mercury in contaminated parts of chemical plants：（应用电子探针定位和物种形成的汞污染地区化工厂）.pdfVIP
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Mikrochim. Acta 125,301-306 (1997)
Mikrochimica Acta
9 Springer-Verlag 1997
Printed in Austria
Application of EPMA to the Localization and Speciation of Mercury
in Contaminated Parts of Chemical Plants*
Ulrich Wendt** and Hartmut Heyse
Department of Materials Science and Materials Testing, Otto-von-Guericke University Magdeburg, Universitaetsplatz 2, D-39106
Magdeburg, Federal Republic of Germany
Abstract. The positions of enrichment of mercury and its com- reduction of the materials volume, it is necessary
pounds in surface layers and within the micro structure of metallic to separate the c ont a m inated materials from the non-
materials originating from closed-down chemical plants were detec-
ted by electron probe microanalysis. Energy dispersive X-ray spec- c ont a m inated parts prior to the d eco n tam ina tio n
trometry is useful for the analysis of mercury. However, the energy process.
resolution is not sufficient for detecting small amounts of sulphur F o r the integral analysis of the mercury content it is
and to measure quantitativelythe chemical bonding state ofmercury
possible to use X-ray fluorescence spectrometry as
as sulphide or chloride. Therefore, it was also necessary to use
a wavelength dispersive X-ray spectrometer. The results show that a solid state me
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