两种离子液体双水相体系萃取葛根素的比较（Comparison of Puerarin extracted by two ionic liquids in aqueous two-phase system）.docVIP

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两种离子液体双水相体系萃取葛根素的比较（Comparison of Puerarin extracted by two ionic liquids in aqueous two-phase system）.doc

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两种离子液体双水相体系萃取葛根素的比较（Comparison of Puerarin extracted by two ionic liquids in aqueous two-phase system）

两种离子液体双水相体系萃取葛根素的比较（Comparison of Puerarin extracted by two ionic liquids in aqueous two-phase system） Comparison of Puerarin extracted by two ionic liquids in aqueous two-phase system Author: Cao Jing, fan Ping, Kong Tao, Zhang Lu [Abstract] Objective To establish [Bmim], BF4/NH4) 2S04 and [Braim] BF4/NaH2P04 two based on room temperature Aqueous two-phase extraction system of ionic liquid / salt and its application in the extraction and separation of Ge Gensu. Methods respectively The two systems were optimized to investigate the amount of ionic liquid, the amount of salt, and the amount of Ge Gensu added Effects of different alcohols on the distribution of Puerarin in two phases. Results were found after optimizing the experimental conditions at most Good condition: (NH4) 2S04 dosage is 0.3, 0.36 g/ml, [Bmim]BF4 dosage is 0.32 0.40 g/ml, the amount of Puerarin solution is 1.5 ml, the amount of ethanol is 2%, the extraction rate of Puerarin can be Reach more than 97%. Conclusion [Bmim]BF4/ (NH4) 2S04 aqueous two-phase system has higher extraction rate than Pueraria lobata, When adding small amount of ethanol, the extraction rate of Puerarin was increased obviously. Keywords ionic liquid; aqueous two-phase system; puerarin; extraction separation; Abstract:ObjectiveTwo, ionic, liquids, aqueous, two-phase, systems Based, on, [Bmim]BF4/ (NH4), 2S04, and, [Bmim]BF4/NaH2P04, were, investigated To, obtain, effective, constituent, puerarin, from, pueraria., Methods Experimental, conditions, of, each, of, these, two, systems, optimized, were, Including, the, amount, of, ionic, liquid, salt, puerarin, and Alcohol., Results, After, optimizing, the, experimental, conditions, the Best, conditions, were, the, amount, of (NH4), 2S04, for, 0., IB, 0%, g/ral, [Bmim]BF4, for 0.32, 0.40, g/ml, adding, 1.5, ML, puerarin, solution, Ethanol at 2%, the, extraction, efficiency, of, puerarin, could,, be, up, to 97%., ConclusionThe, [Bmim]BF4/ (NH4), 2S04, system, has, a, higher, extractio