甘肃不同地区售青黛监督抽验质量考察-中国药事.PDF

362 中国药事 2015 年 4 月 第 29 卷 第 4 期 甘肃不同地区市售青黛监督抽验质量考察 1 2 1* （1. 甘肃省白银市药品检验检测中心，白银 730900；2. 白银市 张富娴 ，侯海功 ，吕益涛 药品稽查局，白银 730922） 摘要 目的 ：对甘肃省不同地区市售的青黛进行监督抽样检验，考察青黛质量。方法：按照《中国药典》 2010 年版一部方法，对从 13 个地州市抽样的 41 批青黛进行性状、理化鉴别，水溶性色素检查，靛蓝、 靛玉红含量检验，并增加了水溶液的酸碱性、脂溶性色素的检查。结果：监督抽检的 41 批青黛样品中 21 批不符合规定，其中 11 批属于劣质品，10 批属于伪制品。结论：建议加强青黛质量监管，规范炮制工 艺，完善质量标准。 关键词： 青黛抽验；中药质量监督；理化鉴别；水溶性色素检查；靛蓝；靛玉红；脂溶性色素检查 中图分类号：R927.1 文献标识码：A 文章编号： 1002-7777(2015)04-0362-07 Evaluation of the Quality of Indigo Naturalis Sold in Different Aeras of Gansu 1 2 1* Zhang Fuxian , Hou Haigong , Lv Yitao Drug Inspection and Testing Center of Baiyin City of Gansu (1. Province, Baiyin 730900, China; 2. Drug Inspection Bureau of Baiyin City of Gansu Province, Baiyin 730922, China ） Abstract Objective: In order to survey the quality of indigo naturalis, evaluation test of 41 batches of indigo naturalis sold in different areas of Gansu was conducted. Methods: The character, physiochemical identification, water soluble pigment check, and contents of indigo as well as indirubin of the 41 batches of indigo naturalis sampled from 13 areas in Gansu were examined and determined according to Chinese Pharmacopoeia (2010 I). Inspection of acid-base aqueous solution and fat soluble pigment was also conducted. Results: The results showed that 21 batches did not meet standards, and among them, 11 batches were bad varieties and 10 batches were adulterant. Conclusion: It is suggested that the quality supervision of indigo naturalis should be strengthened, the processing technology be regulated and the quality standard be improved. Keywords: indigo naturalis sampling inspection; traditional Chinese medicine quality survey; physiochemical identification; water soluble pigment check; indigo; indirubin; fat soluble pigment check