农产品中转基因检测抽样研究-第4部分从批到实验室样品.PDFVIP

7 4 Vol. 7 No. 4 2016 4 Journal of Food Safety and Quality Apr. , 2016 -4 : * 郑 江, 徐 静, 卲筠乔, 张 琳, 曹际娟 , 白 璐, 汪 霖 (, 116001) 摘 要: 目的 , 方法 5 , 395 /, 结果 RSD , 结论 104 , 关键词: ; ; Sampling for genetically modified organism content analysis in agricultural products-part 4: process from lot to laboratory sample * ZHENG Jiang, XU Jing, SHAO Yun-Qiao, ZHANG Lin, CAO Ji-Juan , BAI Lu, WANG Lin (Liaoning Entry-Exit Inspection and Quarantine Bureau , Dalian 116001, China) ABSTRACT: Objective To study the effects of the sub-process from lot to laboratory sampling on the accuracy of results during sampling of genetically modified organism (GMO) content analysis in agricultural products. Methods During 5 years, increments were sampled from 395 batches of bulk lots at ports and analyzed independently. Results Statistical analysis, including the heterogeneity posed by increments, variograph, auxiliary functions and total sampling RSD were obtained to assess the effects of mass, increment number, sampling method and lot size on measuring result. Conclusion For the bulk cargo with GMO content larger than 10-4, minimum increment mass and number, sampling method and lot size were detailed advised. KEY WORDS: genetically modified organisms; sampling; agricultural products