CHEMICAL OXYGEN DEMAND Fisher Scientific（化学需氧量,费舍尔科学）.pdf

CHEMICAL OXYGEN DEMAND Thermo Orion Method CODL00 and CODH00 Revision 5, 03/25/2005 Accepted by U.S. EPA on March 31, 2005 for wastewater compliance monitoring. 1.0 Scope and Applications 1.1 This method is a convenient packaging of the technology in Standard Methods “Chemical Oxygen Demand”, Method 5220 D, “Closed Reflux, Colorimetric Method”.(See Ref. 16.1). It is based on the use of Thermo Orion Test Kits Cat. No. CODL00, or CODH00, or equivalent. The method determines chemical oxygen demand (See Definitions, Section 3.1). Chemical oxygen demand is an aggregate property of water, and no CAS Registry Number is appropriate. 1.2 The method consists of two procedures: the first (“Low Range”) is applicable to natural and treated waters at concentrations from 15 to 150 mg/L COD; and the second (“Mid-Range”) is applicable from 100 to 1500 mg/L COD . Where sample results exceed the applicable range of the method, the sample must be diluted to within the applicable range and reanalyzed. 1.3 This method is for use in the Environmental Protection Agencys (EPAs) data gathering and monitoring programs under the Clean Water Act, the Resource Conservation and Recovery Act, and the Comprehensive Environmental Response, Compensation and Liability Act. 1.4 The MDL for the low range procedure in this method was determined to be 4.6 mg/L COD using an AQUAfast AQ2040 Colorimeter and an COD L00 Test Kit. This value was derived from analysis of 9 aliquots with a concentration of 7 mg/L COD. The MDL for the mid-range procedure was determined to be 16 mg/L, using 9 aliquots with a concentratio