高效液相法测定冠舒片中原儿茶醛含量（Determination of protocatechuic aldehyde in Guanshu tablets by HPLC）.docVIP

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高效液相法测定冠舒片中原儿茶醛含量（Determination of protocatechuic aldehyde in Guanshu tablets by HPLC）.doc

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高效液相法测定冠舒片中原儿茶醛含量（Determination of protocatechuic aldehyde in Guanshu tablets by HPLC）

高效液相法测定冠舒片中原儿茶醛含量（Determination of protocatechuic aldehyde in Guanshu tablets by HPLC） Determination of protocatechuic aldehyde in Guan Shu tablets by HPLC Update Date: 2009-12-21 Click: Zhang Yan, Guo Jianhua, Shao Rongzi, Zhang Hua Abstract: RP HPLC method was used to determine the content of protocatechuic aldehyde in Guan Shu tablets and Radix Salviae miltiorrhizae. In the experiment, Varian KYWG-C18 column was used, with methanol, -0.5% and acetic acid as mobile phase, the average recovery was 98.78%, RSD=1.6%, fast, simple and reproducible, and can be used for the quality control of Guan Shu tablets. Keywords Guan Shu tablet; Radix Salviae Miltiorrhizae; protocatechuic aldehyde; HPLC; The, Determination, of, Protocate, Chualdehyde, in, Teblete, Guanshu, HPLC, by Zhang, Yan, Guo, Jianhua, Shao, Rongzi, et, Al Jinan, General, Hospital, of, PLA, Jinan 250031 Abstract RP-HPLC method was developed for the protocate chualdehyde in Tablete Guanshu. ODS column of Varian KYWG-C18, mobile phase methanol-0.5% acetc acid (70: 10) were employed. The extraction recovery was 98.7% RSD was 1.6%. The method, was simple, rapid and well reproducible and can be used in the quality control. Key, words, Tablete, Guanshu; Danshen; Protocate chualdehyde; HPLC Guanshu tablets is a pure traditional Chinese medicine preparation by the hospitals own production, composed of Radix Salviae Miltiorrhizae, Rhizoma Corydalis, radix puerariae, Yin Chen, the main for the treatment of coronary heart disease, myocardial infarction, curative effect. In order to control the quality of the product, HPLC method was used to determine the content of protocatechuic acid in Radix Salviae Miltiorrhizae, its raw material, Radix Salviae miltiorrhizae. 1 instrument and reagent Type LC-4A high performance liquid chromatograph (SHIMADZU), SPD-2A UV detector, C-R3A data processor; protocatechuic aldehyde (China control of pharmaceutical and Biological Products Institute), Guanshu tablets (homemade), negative con