原创力文档a study on preparation and use of nano poly pyrrole and nano poly (3,4-ethylenedioxythiophene) coated glassy carbon electrode for the determination of antihistamine in pharmaceutical and urine sample英文论文.pdfVIP
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a study on preparation and use of nano poly pyrrole and nano poly (3,4-ethylenedioxythiophene) coated glassy carbon electrode for the determination of antihistamine in pharmaceutical and urine sample英文论文
Materials Sciences and Application, 2011, 2, 957-963 957
doi:10.4236/msa.2011.28128 Published Online August 2011 (http://www.SciRP.org/journal/msa)
A Study on Preparation and Use of Nano Poly
Pyrrole and Nano Poly
(3,4-Ethylenedioxythiophene) Coated Glassy
Carbon Electrode for the Determination of
Antihistamine in Pharmaceutical and Urine
Sample
1* 2 1 3
Balathandapani Muralidharan , Gopalakrishnan Gopu , Saraswathy Laya , Chinnapiyan Vedhi ,
Paramasivam Manisankar2
1Department of Chemistry, Birla Institute of Technology and Science-Pilani, Dubai Campus, Dubai, U.A.E; 2Department of Indus-
trial Chemistry, Alagappa University, Tamilnadu, India; 3Department of Chemistry, V.O. Chidambaram College, Tamilnadu, India.
*
Email: bmuralidharan.bits@
Received September 25th, 2010; revised December 30th, 2010; accepted May 17th, 2011.
ABSTRACT
Pheniramine maleate (PA), an antihistamine, was determined by Differential Pulse Stripping voltammetry using nano
polypyrrole (Ppy) and nano poly (3,4-ethylenedioxythiophene) (PEDOT) modified glassy carbon electrodes. The cyclic
voltammetric behavior of pheniramine was studied in aqueous acidic, neutral and alkaline conditions. One well-defined
oxidation peak was observed in the cyclic voltammograms at all pHs. The influence of pH, scan rate and concentration
revealed irreversible electron transfer and the oxidation was diffusion controlled adsorption. The SEM analysis con-
firmed good accumulation of PA on the electrode surface. A systematic study of influence of various experimental pa-
rameters that affect the stripping voltammetric response was carried out and the maximum peak current conditions
were arrived at. Calibration was made under maximum peak curren
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