电子探针背景扣除和谱线干扰修正方法的进展.pdfVIP

2008 2 Vol. 27, No. 1 February 2008 ROCK AND M INERAL ANALYSIS 4 ~ 54 : 2008) 01004 - 06 电子探针背景扣除和谱线干扰修正方法的进展 1, 2 2* 3 姚 立 , 田 地 , 梁细荣 ( 1. , 130026; 2. , 130061; 3. , 510640) : 对提高电子探针分析精度和分辨本领的关键和难点 背景扣除和 叠峰修正的理 论和方法发展进行了综述介绍了避免谱线干扰的方法和计算谱线干扰量的主要算法及软件应 用效果, 包括估计干扰因子法模拟元素谱图法最小二乘方拟合法及谱线去卷积运算法讨论 了分析中的背景来源及非线性背景扣除的理论和方法发展, 并对背景和谱线干扰修正的发展前 景进行了展望引用文献 62篇 : 电子探针分析; 背景扣除; 谱线干扰修正; 综述 : P575. 1 : A Progress in Background Subtraction and Spectral Interference Correction in Electron ProbeM icroanalysis 1, 2 2* 3 YAO L i , TIAN D i , LIAN GX irong ( 1. CenterofTesting Scientific Expermi en,t Jilin University, Changchun 130026, China; 2. College of Instrumentation Eel ctricalEngineering, Jilin University, Changchun 130061, China; 3. Key Laboratory of Isotope Geochronology and Geochemistry, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China) Abstract: Background subtraction and interference correction are the crucial processes to mi prove the precision and the resolving pow er of the electron m icroprobe analyzer. So the theories and m ethods involved the two processing issues w ere review ed in th is paper. The methods, softw are and correspond ing effects about interference correction w ere summarized, w hich includes the m ethods of estmi ate interference factor, elemental smi ulating spectrum, leastsquare fitting and spectral deconvolution, etc. The emphasis w as focused on the origins of background, as w ell as the development of the theories and method