防感鼻腔喷雾液薄层鉴别（TLC identification of anti flu nasal spray）.docVIP

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防感鼻腔喷雾液薄层鉴别（TLC identification of anti flu nasal spray）.doc

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防感鼻腔喷雾液薄层鉴别（TLC identification of anti flu nasal spray）

防感鼻腔喷雾液薄层鉴别（TLC identification of anti flu nasal spray） TLC identification of anti flu nasal spray Update Date: 2011-04-08 Click: Zhou Yuhong, Wu Jianwei, Dai Hangfeng, Zhang Quanlong Abstract the Anti Sense nasal spray fluid in Astragalus, Folium Isatidis, honeysuckle on TLC, good reproducibility and strong specificity, can be used as one of the quality control of the preparation. Keywords Anti Sense nasal spray; TLC identification; The anti flu nasal spray is developed according to the effective clinical prescription. It has the effect of clearing away heat and toxic substances, and has remarkable effect in preventing influenza and respiratory tract infection. Composed of astragalus root, isatis leaf, honeysuckle and other 5 kinds of Chinese medicine. In order to better control the quality, of which 3 were the main herbs Astragalus, Folium Isatidis, Flos Lonicerae by tlc. 1 instruments and reagents, materials 1.1 instruments: HUV2-3A double wavelength UV fluorescence lamp (Guangzhou Huicheng studio). 1.2 reagent: silica gel G (Qingdao ocean chemical plant); sodium carboxymethyl cellulose (Shanghai chemical reagent purchasing and supply station); polyamide film (Zhejiang Huangyan four biochemical plant material factory). 1.3 materials: anti flu nasal spray and negative contrast liquid (all supplied by the municipal trachea Research Institute); Huang Qijia, indirubin and chlorogenic acid reference (supplied by Chinese pharmaceutical and biological products inspection). 2 thin layer identification 2.1 identification of astragalus root: take the sample 20 ml, set aside liquid funnel, chloroform, n-butanol (1: 1) shake, extract 2 times, 15 times ml/ times. The combined extract, the separating funnel, washed with 1% potassium dihydrogen phosphate solution 2 times, 20 times ml/. Discard the aqueous solution, chloroform - butanol extract in water, steam dry, residue, add methanol 1 ml, dissolve as test sample solution. The negative samples of Astragalus membranaceus were