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D_101_型树脂对芍药苷吸附分离性能的研究
122 Vol. 12,No. 2
20062 Chinese Journal of Experimental Traditional Medical Formulae Feb. ,2006
101
*
桂双英 , 周亚球, 柯仲成
( 安徽中医学院药学院药剂教研室, 安徽 合肥 230031)
[ ] :: HPLC ;
: 101: 25mg
mL36BVh, 322mgg,20%9125%, 7370% : 101
[] ;; ;;
[] R284. 1 [ ] B [ ] 2006
Adsorption and Separation Properties of D101 Resin for Purification of Paeoniflorin
GUI Shuangying, ZHOU Yaqiu , KE Zhongcheng
( School of Pharmacy , Anhui College fo TCM,Hfe ei 230031, China)
[Abstract] Objective:To study the separation effect of 101 macroporous resin for the purification of Paeoniflorin
in Ra ix Paeonia .Methods:HPLC was used to analyze the content of Paeoniflorin, and the adsorption performance and
the elution parameters were investigated.Results:The optimal separation conditions were as follows: the concentration of
Paeoniflorinwas 2. 5mgmL with a flow rate of 3. 6BVh, and 20% alcohol was used as eluant. The adsorption of
Paeoniflorin was 32.2mgg, and the elution ratio of Paeoniflorin was 91.25%, and thepurity of Paeoniflorin reached 73.
70% .Conclusion: 101 resin can be used to refine the Paeoniflorin in the extraction of Ra ix Paeonia.
[Key words] Macroporous resin; Ra ix Paeoniae Rubra; Paeoniflorin; Adsorption; Separation
,, ,, ,
,
, 1
[ 1]
, LC10A ( ) ;
, Paeonia lactfi lora Pall.
(,
[2] [ 1, 3]
, ) ,
, ; 101(
[4]
) ; , ,
101
2
VPO S 46mm 150mm () ; -
[ ]
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