IP143简易手册.docxVIP

IP143 ASTM D6560-00BS 2000-143:2004Determination ofasphaltenes (heptaneinsolubles) in crude petroleum and petroleum products1,Scope测试各种油品（260℃后流出物）中庚烷不能溶解的沥青质。精度范围0.50%m/m到30.00%m/m。油品中含有添加剂可能会引起误差2,Normative references3,Definitions3.1 AsphaltenesWax-free organic material insoluble in heptane,but soluble in hot toluene4 Principle样品混合庚烷，加热回流，蜡状的物质被庚烷溶解，沥青质被甲苯溶解5 Reagents and materials5.1 toluene5.2 Heptane6 Apparatus6.2 Condenser Minimum length 300 mm6.3 Reflux extractor6.4 Conical flasks6.5 stopper6.6 Evaporating vessel6.7 Filter funne6.8 Filter papers6.9Analytical balance6.10 Forceps6.11 Timing device6.12 Oven6.13 Graduated cylinders,50ml,100ml.6.14 stirring rods,150mm by 3mm diameter6.15Cooling vessel6.16 Mixer8, Test portion preparation8.1取样前，要充分摇晃均匀，必要时可以加热，但是不要过80℃8.2 Heat samples of penetration grade bitumensto a temperature notexceeding 120 ℃, and stirwell before taking an aliquot.8.3 Samples of hard bitumens shall be ground toa powder before an aliquot is taken.8.4 Samples of crude petroleum shall beprepared in accordance with theproceduredescribed in annex A, unless it is known that thecrude petroleum contains negligible quantities ofmaterial boiling below 80 ℃9 Apparatus Preparation9.1 Clean all glass flasks (6.3) and dishes (6.6)by a means that matches thecleanliness obtainedby the use of a strongly oxidizing agent such asammonium peroxydisulfate in concentrated sulfuricacid at approximately 8 g/l, or sulfuric acid itself,soaking for at least 12 h, followed by rinses in tapwater, distilled water and then acetone, usingforceps only for handling.9.2 For routine analysis, use a proprietarylaboratory detergent to clean the glassware,followed by the rinses described in 10.1. When thedetergent cleaning no longer matches thecleanliness required based on visual appearance, usea strong oxidizing agent.9.3 After rinsing, place the glassware in theoven (6.12) for 30 min, and cool in the coolingvessel (6.15) for 30 min before weighing..1010.1weigh the quantity,