磁性微球表面光引发聚合制备金属配位印迹层及选择性富集奶样中氟.PDF

磁性微球表面光引发聚合制备金属配位印迹层及选择性富集奶样中氟.PDF

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磁性微球表面光引发聚合制备金属配位印迹层及选择性富集奶样中氟

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 * 张 静, 吕运开 , 于丽青 (, 071002) 摘 要: 目的 , 方法 , -, , 125 W -Co( Ⅱ), 结果 89.6%~100.8%, 1.4%~5.5%, 1.72 μg/kg 5.74 μg/kg, 2.05 μg/kg 6.82 μg/kg, 1.18 μg/kg 3.94 μg/kg结论 关键词: ; ; ; ; Metal complex imprinted layer synthesized by photo-polymerization on surface of magnetic microspheres for selective enrichment of fluoroquinolones residues from milk * ZHANG Jing, LV Yun-Kai , YU Li-Qing (College of Chemistry and Environmental Science, Hebei University, Baoding 071002, China) ABSTRACT: Objective To develop a preparation method of metal coordination imprinted magnetic microspheres for selective enrichment of fluoroquinolones drug residues from milk. Methods The magnetic microspheres were synthesized by the solvothermal method, and was coated with silica gel, the iniferter was synthesized on surface of the magnetic silica microspheres, and then enrofloxacin–Co( Ⅱ) coordination imprinted layer was synthesized under an ultraviolet spotlight of 125 W. The obtained sorbents were used for magnetic

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