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土壤全氮测定(半微量开氏法)(Determination of total nitrogen in soil (semi micro Kjeldahl method))
土壤全氮测定(半微量开氏法)(Determination of total nitrogen in soil (semi micro Kjeldahl method))
Determination of soil total nitrogen (semi micro Kjeldahl method).Txt - you pedal both boats, you row really beautiful. Every man who says he doesnt want to be in love has an impossible man in his heart. I love every unhappy but still laughing child. (there is no one, see through me, invisible, know Im waiting for someone). Peoples Republic of China national standard
Soil total nitrogen method
(half trace Kjeldahl method)
Method for the determination
Of soil total nitrogen
(Semi-micro, Kjeldahl, method)
UDC 631.423
GB 717387
This standard is applicable to the determination of soil total nitrogen content.
1 scope of application
When the sample is under the influence of accelerator, the organic compounds with various nitrogen compounds are decomposed into ammonium nitrogen by complex reaction at high temperature. The ammonia distilled after alkalization is absorbed by boric acid, and the total nitrogen content of the soil (excluding all nitrate nitrogen) is determined by acid standard solution.
Including total nitrogen nitrate and nitrite nitrogen determination in sample digestion, Potassium Permanganate will need to use nitrite oxidation in samples of nitrate nitrogen, then all the reduction of iron nitrate reduction, converted to ammonium nitrogen.
2 instruments and equipment
2.1 soil sample shredder;
2.2 agate mortar;
2.3 soil sieve: aperture 1.0mm (18 mesh); 0.25mm (60 mesh);
2.4 analysis balance: 0.0001g.
2.5 hard fused flasks: Volume 50ml, 100ml;
2.6 semi micro fixed nitrogen distillation unit;
2.7 half a tube: Volume 10ml, 25ml;
2.8 cone flask: Volume 150ml;
2.9 electric furnace: 300W variable temperature furnace.
3 reagent
3.1 sulfuric acid (GB 62577): chemical pure;
3.2 sulfuric acid (GB 625-77) or hydrochloric acid (GB 622-77): analysis of pure, 0.005mol/L sulfuric acid or 0.01mol/L hydrochloric acid standard solution;
3.3 sodium hydroxide (GB 62981): industrial or chemical
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