(2e,2e)-3,3-(1,4-phenylene)bis[1-(2,5-dimethyl-3-thienyl)prop- 2-en-1-one](2 e 2本部)3,3 -(1,4-phenylene)bis[1 -(2,5-dimethyl-3-thienyl)道具2-en-1-one].pdfVIP

下载本文档

8
0
约6.85千字
约 3页
2017-11-02 发布于上海
举报
版权申诉

(2e,2e)-3,3-(1,4-phenylene)bis[1-(2,5-dimethyl-3-thienyl)prop- 2-en-1-one](2 e 2本部)3,3 -(1,4-phenylene)bis[1 -(2,5-dimethyl-3-thienyl)道具2-en-1-one].pdf

1、本文档共3页，可阅读全部内容。
2、原创力文档（book118）网站文档一经付费（服务费），不意味着购买了该文档的版权，仅供个人/单位学习、研究之用，不得用于商业用途，未经授权，严禁复制、发行、汇编、翻译或者网络传播等，侵权必究。
3、本站所有内容均由合作方或网友上传，本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺！文档内容仅供研究参考，付费前请自行鉴别。如您付费，意味着您自己接受本站规则且自行承担风险，本站不退款、不进行额外附加服务；查看《如何避免下载的几个坑》。如果您已付费下载过本站文档，您可以点击这里二次下载。
4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等，请点击“版权申诉”（推荐），也可以打举报电话：400-050-0827(电话支持时间：9:00-18:30)。
5、该文档为VIP文档，如果想要下载，成为VIP会员后，下载免费。
6、成为VIP后，下载本文档将扣除1次下载权益。下载后，不支持退款、换文档。如有疑问请联系我们。
7、成为VIP后，您将拥有八大权益，权益包括：VIP文档下载权益、阅读免打扰、文档格式转换、高级专利检索、专属身份标志、高级客服、多端互通、版权登记。
8、VIP文档为合作方或网友上传，每下载1次，网站将根据用户上传文档的质量评分、类型等，对文档贡献者给予高额补贴、流量扶持。如果你也想贡献VIP文档。上传文档

(2e,2e)-3,3-(1,4-phenylene)bis[1-(2,5-dimethyl-3-thienyl)prop- 2-en-1-one](2 e 2本部)3,3 -(1,4-phenylene)bis[1 -(2,5-dimethyl-3-thienyl)道具2-en-1-one]

Molbank 2009, M636 OPEN ACCESS molbank ISSN 1422-8599 /journal/molbank Short Note (2E,2E)-3,3-(1,4-Phenylene)bis[1-(2,5-dimethyl-3-thienyl)prop- 2-en-1-one] Abdullah M. Asiri * and Salman A. Khan Chemistry Department, Faculty of Science, King Abdul Aziz University, P.O. Box 80203, Jeddah 21589, Saudi Arabia * Author to whom correspondence should be addressed; E-Mail: aasiri2@.sa; Tel.: +966 2 6952293; Fax: +966 2 6952292. Received: 27 August 2009 / Accepted: 26 October 2009 / Published: 28 October 2009 Abstract: A bis-chalcone has been synthesized by reaction of 3-acetyl-2,5-dimethyl- thiophene and terephthalaldehyde in ethanolic NaOH at room temperature: (2E,2E)-3,3- (1,4-phenylene)bis[1-(2,5-dimethyl-3-thienyl)prop-2-en-1-one] (3) was obtained in high 1 yield. The structure of this compound was established by elemental analysis, IR, H NMR, 13C NMR and EI-MS spectral analysis. Keywords: chalcone; aldol condensation; terephthalaldehyde Aldol condensations are important in organic synthesis, providing a good way to form α,β-unsaturated ketones known as chalcone [1]. Naturally occurring as well as synthetic chalcones are important for their biological activities. Compounds with α,β-unsaturated ketones have become of much interest in recent years on account of their antioxidant [2], antibacterial [3], antidepressant [4], antihypertensive [5] and