highly efficient procedure for the synthesis of fructone fragrance using a novel carbon based acid高效的合成过程fructone香水使用一种新颖的基于碳的酸.pdfVIP

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highly efficient procedure for the synthesis of fructone fragrance using a novel carbon based acid高效的合成过程fructone香水使用一种新颖的基于碳的酸.pdf

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highly efficient procedure for the synthesis of fructone fragrance using a novel carbon based acid高效的合成过程fructone香水使用一种新颖的基于碳的酸

Molecules 2010, 15, 5369-5377; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Article Highly Efficient Procedure for the Synthesis of Fructone Fragrance Using a Novel Carbon based Acid 1 1 2 2 2 Baowei Hu , Chunqing Li , Sheng-Xian Zhao , Lin-Mei Rong , Shao-Qin Lv , Xuezheng Liang 1,* and Chenze Qi 1,* 1 Shaoxing University, Shaoxing, 312000, China 2 Esteve Huayi Pharmaceutical Co., LTD., Shaoxing, 312000, China * Authors to whom correspondence should be addressed; E-Mail: xzliang@ (X.Z.L.); qichenze@ (C.Z.Q.); Tel.: +86-575 Fax: +86-575 Received: 1 June 2010; in revised form: 21 July 2010 / Accepted: 26 July 2010 / Published: 5 August 2010 Abstract: The novel carbon based acid has been synthesized via one-step hydrothermal carbonization of furaldehyde and hydroxyethylsulfonic acid. A highly efficient procedure for the synthesis of fructone has been developed using the novel carbon based acid. The results showed that the catalyst possessed high activity for the reaction, giving a yield of over 95%. The advantages of high activity, stability, reusability and low cost for a simple synthesis procedure and wide applicability to various diols and β-keto esters make this novel carbon based acid one of the best choices for the reaction. Keywords: novel carbon based acid; fructone; synthesis 1. Introduction Acid catal