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study on the xps-esca of aluminum phosphide products研究xps-esca磷化铝产品
Int. J. Mol. Sci. 2005, 6, 198–202
International Journal of
Molecular Sciences
ISSN 1422-0067
© 2005 by MDPI
/ijms/
Study on the XPS-ESCA of Aluminum Phosphide Products
Canping Pan *, Weixi Li and Shuren Jiang
College of Applied Chemistry, China Agricultural University, Beijin 100094, China
Tel.: (+86(10) Fax: +86 (10) URL: /lxy
*Author to whom correspondence should be addressed. E-mail: campingp@;
Received: 1 August 2004 / Accepted: 18 May 2005 / Published: 25 May 2005
Abstract: XPS-ESCA analysis showed small signal for phosphorus in fresh specimens of
aluminum phosphide (AlP). After removal of a layer of about 0.5 – 1.0 µm by argon ion
sputtering, it was observed that signal intensities from oxygen and aluminum increased. The
oxygen signal decreased as a function of sputtering time, synchronously with the increase of
the phosphorous signal from the AlP nucleus. The aluminum signal, which was considered
to be mainly due to AlP and Al(OH) , remained constant. Other impurity elements including
3
N, Mg, etc., were identified in the technical 85% AlP and AlP tablet formulated products.
Keywords: XPS, ESCA, aluminum phosphide.
Introduction
X-ray Photoelectron Spectroscopy (XPS) is a technique for determining the binding energies of
core-electrons [1]. The ESCA spectrum measures the kinetic energies of electrons ejected from a
molecule by
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