synthesis and antimicrobial studies of some novel bis-[1,3,4]thiadiazole and bis-thiazole pendant to thieno[2,3-b]thiophene moiety合成和抗菌研究的一些新颖的双(1,3,4)和bis-thiazole吊坠thieno一种新型润滑脂添加剂噻二唑衍生物[2,3 b]噻吩一半.pdfVIP
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synthesis and antimicrobial studies of some novel bis-[1,3,4]thiadiazole and bis-thiazole pendant to thieno[2,3-b]thiophene moiety合成和抗菌研究的一些新颖的双(1,3,4)和bis-thiazole吊坠thieno一种新型润滑脂添加剂噻二唑衍生物[2,3 b]噻吩一半
Int. J. Mol. Sci. 2012, 13, 3661-3670; doi:10.3390/ijm
OPEN ACCESS
International Journal of
Molecular Sciences
ISSN 1422-0067
/journal/ijms
Article
Synthesis and Antimicrobial Studies of Some Novel
Bis-[1,3,4]thiadiazole and Bis-thiazole Pendant to
Thieno[2,3-b]thiophene Moiety
Nabila Abdelshafy Kheder 1,2 and Yahia Nasser Mabkhot 3,*
1 Department of Chemistry, Faculty of Science, Cairo University, Giza 12613, Egypt;
E-Mail: nabila_abdelshafy@
2 On leave to Department of Pharmaceutical Chemistry, Faculty of Pharmacy, King Khalid
University, P. O. Box 418 Abha 61431, Saudi Arabia
3 Department of Chemistry, Faculty of Science, King Saud University, P. O. Box 2455 Riyadh 11451,
Saudi Arabia
* Author to whom correspondence should be addressed; E-Mail: yahia@.sa;
Tel.: +966-1467-5898; Fax: +966-1467-5992.
Received: 16 January 2012; in revised form: 7 March 2012 / Accepted: 13 March 2012 /
Published: 19 March 2012
Abstract: The synthetic utility of 3,3’-(3,4-dimethylthieno[2,3-b]thiophene-2,5-diyl)bis
(3-oxopropanenitrile) (1) in the synthesis of some novel bis-[1,3,4-thiadiazole] 6a–g and
bis-thiazole 10 and 13 derivatives with thieno[2,3-b]thiophene moiety is reported.
Antimicrobial evaluation of some selected examples from the synthesized products was
carried out and showed promising results.
Keywords: thieno[2,3-b]thiophene; nucleophilic addition; hydrazonoyl halides;
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