synthesis and antimicrobial studies of some novel bis-[1,3,4]thiadiazole and bis-thiazole pendant to thieno[2,3-b]thiophene moiety合成和抗菌研究的一些新颖的双(1,3,4)和bis-thiazole吊坠thieno一种新型润滑脂添加剂噻二唑衍生物[2,3 b]噻吩一半.pdfVIP

synthesis and antimicrobial studies of some novel bis-[1,3,4]thiadiazole and bis-thiazole pendant to thieno[2,3-b]thiophene moiety合成和抗菌研究的一些新颖的双(1,3,4)和bis-thiazole吊坠thieno一种新型润滑脂添加剂噻二唑衍生物[2,3 b]噻吩一半.pdf

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synthesis and antimicrobial studies of some novel bis-[1,3,4]thiadiazole and bis-thiazole pendant to thieno[2,3-b]thiophene moiety合成和抗菌研究的一些新颖的双(1,3,4)和bis-thiazole吊坠thieno一种新型润滑脂添加剂噻二唑衍生物[2,3 b]噻吩一半

Int. J. Mol. Sci. 2012, 13, 3661-3670; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article Synthesis and Antimicrobial Studies of Some Novel Bis-[1,3,4]thiadiazole and Bis-thiazole Pendant to Thieno[2,3-b]thiophene Moiety Nabila Abdelshafy Kheder 1,2 and Yahia Nasser Mabkhot 3,* 1 Department of Chemistry, Faculty of Science, Cairo University, Giza 12613, Egypt; E-Mail: nabila_abdelshafy@ 2 On leave to Department of Pharmaceutical Chemistry, Faculty of Pharmacy, King Khalid University, P. O. Box 418 Abha 61431, Saudi Arabia 3 Department of Chemistry, Faculty of Science, King Saud University, P. O. Box 2455 Riyadh 11451, Saudi Arabia * Author to whom correspondence should be addressed; E-Mail: yahia@.sa; Tel.: +966-1467-5898; Fax: +966-1467-5992. Received: 16 January 2012; in revised form: 7 March 2012 / Accepted: 13 March 2012 / Published: 19 March 2012 Abstract: The synthetic utility of 3,3’-(3,4-dimethylthieno[2,3-b]thiophene-2,5-diyl)bis (3-oxopropanenitrile) (1) in the synthesis of some novel bis-[1,3,4-thiadiazole] 6a–g and bis-thiazole 10 and 13 derivatives with thieno[2,3-b]thiophene moiety is reported. Antimicrobial evaluation of some selected examples from the synthesized products was carried out and showed promising results. Keywords: thieno[2,3-b]thiophene; nucleophilic addition; hydrazonoyl halides;

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