原创力文档textural characterization and energetics of porous solids by adsorption calorimetry结构特征和能量的多孔固体吸附量热法.pdfVIP
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textural characterization and energetics of porous solids by adsorption calorimetry结构特征和能量的多孔固体吸附量热法
Energies 2011, 4, 928-947; doi:10.3390/en4060928
OPEN ACCESS
energies
ISSN 1996-1073
/journal/energies
Article
Textural Characterization and Energetics of Porous Solids by
Adsorption Calorimetry
Vanessa Silenia Garcia-Cuello 1, Liliana Giraldo 1 and Juan C. Moreno-Pirajan 2,*
1 Department of Chemistry, Faculty of Science, National University of Colombia, Bogota, Colombia;
E-Mails: vgarcia@.co (V.S.G.-C.); lgiraldogu@.co (L.G.)
2 Research Group on Porous Solids and Calorimetry, Department of Chemistry, Faculty of Science,
University of the Andes, Bogota, Colombia
* Author to whom correspondence should be addressed; E-Mail: jumoreno@.co;
Tel.: +571-3394949; Fax: +571-3324366.
Received: 20 February 2011; in revised form: 13 April 2011 / Accepted: 28 April 2011 /
Published: 10 June 2011
Abstract: An adsorption microcalorimeter was designed and built in our laboratory and
used for the determination of differential adsorption heats in different samples of porous
solids: activated carbon granules, activated carbon pellets, an activated carbon monolith
and a zeolite sample. This work shows the relationship between adsorption heat and the
pore size of different porous solids using adsorption of NH , CO and N O. The result
3 2
shows that the thermal effect can be related with textural properties and superficial
chemical groups of
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