using hydrophilic ionic liquid, [bmim]bf4 – ethylene glycol system as a novel media for the rapid synthesis of copper nanoparticles使用亲水离子液体[bmim]bf4 -乙二醇系统作为一种新型媒体的快速合成铜纳米粒子.pdfVIP

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using hydrophilic ionic liquid, [bmim]bf4 – ethylene glycol system as a novel media for the rapid synthesis of copper nanoparticles使用亲水离子液体[bmim]bf4 -乙二醇系统作为一种新型媒体的快速合成铜纳米粒子.pdf

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using hydrophilic ionic liquid, [bmim]bf4 – ethylene glycol system as a novel media for the rapid synthesis of copper nanoparticles使用亲水离子液体[bmim]bf4 -乙二醇系统作为一种新型媒体的快速合成铜纳米粒子

Using Hydrophilic Ionic Liquid, [bmim]BF4 – Ethylene Glycol System as a Novel Media for the Rapid Synthesis of Copper Nanoparticles 1 1 1 2 1 Manika Dewan , Ajeet Kumar , Amit Saxena , Arnab De , Subho Mozumdar * 1 Department of Chemistry, University of Delhi, Delhi, India, 2 Department of Microbiology and Immunology, Columbia University Medical Centre, New York, New York, United States of America Abstract In this work, we present a novel method for the synthesis of copper nanoparticles. We utilize the charge compensatory effect of ionic liquid [bmim]BF4 in conjunction with ethylene glycol for providing electro-steric stabilization to copper nanoparticles prepared from copper sulphate using hydrazine hydrate as a reducing agent. The formed copper nanoparticles showed extended stability over a period of one year. Copper nanoparticles thus prepared were characterized by powder X-ray diffraction measurements (pXRD), transmission electron microscopy (TEM) and quasi elastic light scattering (QELS) techniques. Powder X-ray diffraction (pXRD) analysis revealed relevant Bragg’s reflection for crystal structure of copper. Powder X-ray diffraction plots also revealed no oxidized material of copper nanoparticles. TEM showed nearly uniform distribution of the particles in methanol and confirmed by QELS. Typical applications of copper nanoparticles include uses in conductive films, lubrication and nanofluids. Currently efforts are under way in our laboratory for using these nanoparticles as catalysts for a variety of organic reactions. Citation: Dewan M, Kumar A, Saxena A, De A, Mozumdar S (2012) Using Hydrophilic Ionic Liquid, [bmim]BF4 – Ethylene Glycol System as a Novel Media for