有机化合物熔点和沸点的测定（Determination of melting point and boiling point of organic compounds）.docVIP

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有机化合物熔点和沸点的测定（Determination of melting point and boiling point of organic compounds）.doc

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有机化合物熔点和沸点的测定（Determination of melting point and boiling point of organic compounds）

有机化合物熔点和沸点的测定（Determination of melting point and boiling point of organic compounds） Question 1: what happens if the capillary is not sealed? Question 2: why should a clean surface dish be used? Question 3: if the sample in the sample tube is not compacted, what is the effect on the result? Question 4: why can use liquid paraffin as the bath? Question 5: where should a rubber band be located? Why? Question 6: how to control the flame temperature? Question 7: when approaching the melting point, why should the heating rate be controlled very slowly? Such as warming too fast, what is the impact? Question 8: is it possible to use second organic compounds that have been fused for the first time after measuring the melting point? Why ? Question 9: if the sample to be obtained is too small or too small, what is the effect on the measurement result? Thinking question answer: Thinking 1 answer: there will be liquid paraffin into the capillary, affect the observation of solid melting. Question 2 answer: prevent impurities mixed into the capillary so that the melting point is not accurate. Question 3 answer: the melting of solid matter is not complete, affecting the observation of the melting process and melting point judgment. Thinking 4 answer: liquid paraffin boiling point higher. Question 5: a rubber ring to the top in the bath. If it is below the liquid level, the rubber band expands as the temperature increases, The capillary will fall off and cause the experiment to fail. Question 6 answer: alcohol lamp from time to time, suspended heating. Think 7 answer: if the temperature is too fast, it will cause the material to melt rapidly and can not observe the melting point distance. Think 8 questions: No, this is because the first time after the melting point, sometimes some substances will produce partial decomposition, some will Change into other crystalline forms with different melting points. Thinking 9 answer: if the sample to be taken too much, the internal pressure of