核磁共振波谱法（Nuclear magnetic resonance spectroscopy）.docVIP

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核磁共振波谱法（Nuclear magnetic resonance spectroscopy）.doc

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核磁共振波谱法（Nuclear magnetic resonance spectroscopy）

核磁共振波谱法（Nuclear magnetic resonance spectroscopy） Nuclear magnetic resonance spectroscopy I. teaching content 1. the concept of nuclear magnetic resonance spectroscopy 2. the basic principle of nuclear magnetic resonance spectroscopy (spin and magnetic nuclei from NMR generation and related expressions and significance, saturated and famous) 3. structure and proton NMR spectra of organic compounds (chemical shift, spin coupling and splitting, first order spectra and complex patterns, chemical exchange, resonance absorption intensity) Structure and proton nuclear magnetic resonance spectroscopy of 4. organic compounds 5. nuclear magnetic resonance spectrometer 6. basic applications of nuclear magnetic resonance spectroscopy Two. Key and difficult points 1. the conditions and basic principles of nuclear magnetic resonance and the significance of expression 2. various factors affecting the chemical shift 3. mechanism of spin coupling and splitting Splitting law of 4. level spectrum and its application Analysis and structure analysis of 5. spectra Three. Teaching requirements 1., more firmly grasp the conditions and basic principles of nuclear magnetic resonance generation 2. deeper into the concept of dissociation, chemical shift, causes, expressions and influencing factors 3. grasp the proton chemical shift of some common groups 4. general understanding of the concept of complex maps, classification of spin systems and simplification of complex maps Four. Class arrangement is 3 hours Section 1 basic principles of nuclear magnetic resonance Nuclear spin If the nucleus has a spin, it produces a magnetic moment of the nucleus: Spin angular momentum: Nuclear magnetic moment I: spin quantum number; H: Planck constant; nuclear magnetic unit (=eh/2M, c) The spin quantum number (I) is not zero, and the nucleus has a magnetic moment. The spin of the atom can be characterized by (I): Mass number, atomic number, spin quantum number, I Even number 0 Even odd numbers 1, 2, 3... . O