氨咖黄敏胶囊（Paracetamol,Caffein ,Atificial Cow-bezoar and chlorphenamine Maleate capsules）.docVIP

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氨咖黄敏胶囊（Paracetamol,Caffein ,Atificial Cow-bezoar and chlorphenamine Maleate capsules）.doc

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氨咖黄敏胶囊（Paracetamol,Caffein ,Atificial Cow-bezoar and chlorphenamine Maleate capsules）

氨咖黄敏胶囊（Paracetamol,Caffein ,Atificial Cow-bezoar and chlorphenamine Maleate capsules） Paracetamol Caffein Atificial Cow-bezoar and Chlorphenamine Malate Capsules (Suxiaoshangfeng capsule), the main component of acetaminophen, the current standard application of external indicator method (diazotization titration method) determination of the product of the content of paracetamol, the spectrophotometric method for the determination of the content of paracetamol by UV, with satisfactory results. 1 instrument and reagent Ultraviolet spectrophotometer (UV-1601, Japan, SHIMADZU), electronic analytical balance (GR - 200, Japanese SHIMADZU, AR - 135, Shanghai). Paracetamol Caffein Atificial Cow-bezoar and Chlorphenamine Malate Capsules (commercially available products, specifications: each containing 250mg paracetamol, caffeine and Chlorphenamine Maleate in 15mg, 1mg, 10mg (batch number: artificial bezoar; Zheng Kangli Pharmaceutical Co. Ltd. (Guangdong), Dong Kang Pharmaceutical Co. Ltd. (Guangdong), Yili Pharmaceutical Co., Ltd)), acetaminophen control goods (Chinese Institute for drug control; batch number:). Sodium hydroxide was used as the analytical reagent, and water as the purified water for the experiment. 2 methods and results 2.1 solvent The solvent of Paracetamol Tablets content (water and 0.4% NaOH solution) was chosen as the solvent of the experiment. 2.2 preparation of reference solution The precision of acetaminophen control 40mg, into a 250ml volumetric flask, adding 0.4% 50ml of sodium hydroxide and water 50ml 15min, shaking; dissolve acetaminophen, add water to the scale, shake, precise amount of 5ml; the 100ml volumetric flask, add 0.4% 10ml sodium hydroxide solution, add water to the scale, shake as the reference solution. 2.3 preparation of test sample solution Take Paracetamol Caffein Atificial Cow-bezoar and Chlorphenamine Malate Capsules 20 capsules, according to the amount of capsule loading difference Inspection under item, The average grain weight