泡沫吸附法测定金（Determination of gold by foam adsorption method）.docVIP

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泡沫吸附法测定金（Determination of gold by foam adsorption method）.doc

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泡沫吸附法测定金（Determination of gold by foam adsorption method）

泡沫吸附法测定金（Determination of gold by foam adsorption method） Determination of gold, 2006-11-10, 9:50:49, China beneficiation technology network by bubble absorption method; 3030 times, I will compare two methods of foam absorption, and the colorimetric colorimetric determination of gold Method summary The sample was dissolved by HCl and HNO3, and polyurethane foam was used to adsorb Au. In the presence of mixed masking agent, Au was determined by TMK colorimetric method. The method is suitable for determination of omega (Au) /10-6=0.0005~0.5 in geological and geochemical samples. Two. Reagent preparation Mixed masking agent: 100mL, add citric acid ammonium salt, 30g six times methyl four amine, 10gEDTA two sodium salt and 40mL glacial acetic acid in water, and then add 430mL water and mix thoroughly when 40g is dissolved completely. Gold standard solution: take 100mg (accurate to 0.01mg) spectrum pure Au, dissolve in 100mL, Wang Shuizhong, after cooling, water into 1000mL volume bottle, and dilute to calibration, shake. This is a storage solution containing 100 g/mLAu, diluted with HCI (1+99) to prepare the standard solution for Au with a mass concentration of 10 g/mL, 1 g/mL and 0.1 g/mL. Polyurethane foam: take commercially available colorless and porous foam, cut into 0.9 * 0.45 * 5cm strips, soak in HCl (5+95) for 3h or more, rinse with slurry, squeeze dry, and reserve after drying. Three, analysis steps A sample of 10G (accurate to 0.1g) 0.074mm is taken in a 30mL porcelain crucible and burned above 1.5h in a 650~700 high temperature furnace. Take out the cooling and transfer the sample to the 300mL cone. Wet the sample with water and add 30mLHCl and 10mLHNO3 to keep the micro boiling 30min on the electric plate. Take off, add 70mL water, put in 1 foam plastics, cover the bottle stopper, and cone the flask on the shaker, shake 70min or so (middle hand 2~3 times). Remove foam strips, rinse with tap water and press dry. Wrapped in filter paper, the blister is placed