衄咽胶囊渗漉提取工艺优选的研究(Study on the pharyngeal bleeding capsule percolation extraction process optimization).docVIP
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衄咽胶囊渗漉提取工艺优选的研究(Study on the pharyngeal bleeding capsule percolation extraction process optimization)
衄咽胶囊渗漉提取工艺优选的研究(Study on the pharyngeal bleeding capsule percolation extraction process optimization)
Study on the pharyngeal bleeding capsule percolation extraction process optimization
Update Date: 06-04: Tang Tang, Chen Longhui, Tang Shanshan, Yang Jiefang, Zhang Dan, LAN Cai, Li Jian, Ceng Xiaoxia
[Key words] bleeding throat capsule; percolation;,,,, baicalin,,
Abstract: Objective To establish a method for extraction of pharyngeal capsule bleeding hemostasis of baicalin. Methods with baicalin as index by orthogonal design method, using UV visible light spectrophotometer, the bleeding throat capsule percolation extraction process were optimized. The results of adding 6 times amount of 80% ethanol in medicine, soaking for 24 h, 96 h percolation, the yield of baicalin reached (12.24 + 2.691)%; RSD=1.18% stability test; precision RSD=0.788% (n=6); recovery experiment, the average recovery was 98.9%, RSD=1.10%. Conclusion the optimum percolation extraction process is stable and feasible.
Keywords: bleeding throat capsule; percolation method; baicalin
Research on the Percolation Extract Process of N Yan Capsules
Abstract:ObjectiveTo establish the Percolation Extract Method of N Capsules.MethodsBy the orthogonal design and Yan Ultraviolet-visible absorption spectrophotometry, taking the gain rate of Baicalin as the index.The Percolation extract process was optimized.ResultsThe factors influencing the alcohol-percolation were as follows:6 times amount of 80% alcohol was added, soaked for 24hours and percolated for 96hours, the gain rate of baicalin came up to (12.24 + 2.691)%; the RSD% of precision experiments (baicalin) was 0.788 (n=6); the average recovery of baicalin was 98.9%, RSD% was 1.10; the RSD% of stabilize experiments (baicalin) was 1.18.ConclusionThe optimized process is stable and feasible.
Key words:N Yan Capsules Percolation; extract method; Baicalin
As the experience of pharyngeal bleeding capsule deputy director of Department of ENT physician Chen Longh
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