电位滴定法测定酱油中氯化钠含量（Determination of sodium chloride in soy sauce by potentiometric titration）.docVIP

电位滴定法测定酱油中氯化钠含量（Determination of sodium chloride in soy sauce by potentiometric titration） The standard solution records the primary electricity Two standard commercial solution is used to determine the amount of standard solution at the end of the titration , , Bit values continued to titrate until the potential value changed little Learn scriptures , C. Burned for an hour of sodium chloride standard solution Dissolve in a suitable amount of water and settle until Standard solution dosage accurate , Draw a titration Line ,. The end-point potential value is obtained at the end of titration For official measurement , Be sure to absorb water and dilute it to Standard solution Direct standard solution Write down Titrate to the above specified standard solution , Standard solution , The amount of liquid used for result calculation and blank test Blank background indicator method , Weigh , . , Dissolve with water and dilute until , When stored in brown bottles, according to the literature Method mark Quasi dilution plus Samples of soy sauce are accurately absorbed , Make sure the standard solution is absorbed , Dilute with water until to Accurately absorb this sample , White porcelain evaporating dish standard solution Draw , Water and , Indicator in standard solution , Dilute with water until , The bar is stirred and titrated with liquid until it is orange , The standard solution is determined by the following potentiometric titration The results are consistent with only the silver electrode and the type acidity meter , Standard solution The same amount of liquid as a blank test blank background value type double saltbridge calomel Burette , Results and discussion Potentiometric titration curve The outer electrode of the bridge is saturated solution Reagents used and , Water is pure and deionized water A potentiometric titration diagram obtained from the determination of the sample It is obvious that the abrupt rise of titration to the end point is obvious , Experimen