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顶空气相色谱法快速测定食用植物油中有机溶剂残留量的研究
6 2 Vol. 6 No. 2
2015 2 Journal of Food Safety and Quality Feb. , 2015
*
王永芳 , 葛含光, 王利强, 葛宝坤
(, 300461)
摘 要: 目的 方法
, , , ,
, 结果 2 mg/kg~200 mg/kg , ,
Y=17.4427X +44.4790, R²=0.9999 99.1%~105.0%,
3.0%结论 , ,
关键词: ; ;
Study on rapid determination of residual solvents in edible vegetable oils by
headspace gas chromatography
WANG Yong-Fang, GE Han-Guang, WANG Li-Qiang, GE Bao-Kun
(Animal, Plant and Foodstuffs Inspection Center , Tianjin Entry-Exit Inspection and Quarantine Bureau, Tianjin 300461,
China)
ABSTRACT: Objective To establish a method to determine the residual solvents in edible vegetable oils by
headspace gas chromatography. Methods The equilibrium temperature and equilibrium time were discussed.
Residual solvents were separated completely by the optimized method and matrix effects were reduced. By
recording the peak area of each component, the results were quantified by normalization method. Results The
linear relationship was good from 2 mg/kg to 200 mg/kg, and the linear equation was Y=17.4427X +44.4790,
R²=0.9999. The additive recovery was 99.1%~105.0% and the coefficient of variation was less than 3.0%.
Conclusion This method is easier, faster and suitable for the determination of residual
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