苦楝花挥发油GC-MS 分析.pdfVIP

食品与药品 Food and Drug 2010年第 12卷第03期 99 苦楝花挥发油GC-MS分析 1 1 2* 1 1 丁凤伟 ，彭艳丽 ，李 明 ，彭慧敏 ，牟宗慧 （1. 山东中医药大学，山东 济南，250355；2 ．济南卫生学校，山东 济南 250022 ） 摘 要：目的 分析比较苦楝花挥发油的化学成分。方法 用气-质联用 （GC-MS ）技术分析。结果 分离出苦楝花挥发油74 种成分，其中确定了63种化合物。结论 苦楝花挥发油以饱和烷烃为主，相对含量最高的是十六碳酸，占7.984 %，相对含 量最低的是二十八烷，占0.393 % 。这与此前报道不同。苦楝不同部位的挥发性成分相差较大，综合开发利用苦楝时应分 部位提取。 关键词：苦楝花；气-质联用；挥发油 中图分类号：R931.71 文献标识码：A 文章编号：1672-979X(2010)03-0099-04 Analysis on Volatile Oil of Melia azedarach Flowers by GC/M S 1 1 2 1 1 DING Feng-wei , PENG Yan-li , LI Ming , PENG Hui-min , MU Zong-hui (1. Shandong University of Traditional Chinese Medicine, Jinan 250355, China; 2. Jinan Health School, Jinan 250022, China) Abstract: Objective To analyze the constituents of volatile oils of Melia azedarach flowers. Methods The gas chromatography-mass spectrometry (GC/MS) method was adopted. Results Seventy-four components of volatile oils were isolated and obtained. Among them, sixty-three components were identified. Conclusion The volatile components of Melia azedarach flowers are mainly saturated alkanes, including hexadecanoic acid with the highest relative amount of 7.984 ％ and octacosane with the lowest relative amount of 0.393 ％. This differs from the results in the previous report. The volatile components in different parts of Melia azedarach are also significantly different. Melia azedarach can be extracted and utilized on the basis of different parts. Key Words: Melia azedarachflowers ；GC/MS；volatile oil 苦楝花为楝科植物楝M elia agedarach L. 的干燥 发利用提供理论基础与科学依据。 花 。苦楝是古老的树种，我国公元6世纪 《齐 民要 1 材料、仪器与试剂 术》中就有楝树生长特性及育苗造林的记载。我国 1.1 材料