陶瓷uo2孔隙率与孔隙分布的定量测量-中南大学学报.pdfVIP

第 38 卷第 3 期 中南大学学报( 自然科学版) Vol.38 No.3 2007 年 6 月 J. Cent. South Univ. (Science and Technology) Jun. 2007 陶瓷UO2 孔隙率与孔隙分布的定量测量 黄志锋，禇胜林，廖寄乔，普建强，郑灵芝 ( 中南大学 粉末冶金国家重点实验室，湖南 长沙，410083) 摘 要：借助大型金相显微镜，对陶瓷 UO2 的孔隙率与孔隙分布金相定量测量进行研究。研究结果表明：利用组 合物镜(100 ×，50 ×，20 ×，5 ×)测量陶瓷 UO2 的孔隙率与孔隙分布比利用单个物镜(20 ×)测量所得结果精度高， 分布曲线更光滑；利用低倍物镜(20 ×，10×，5 ×)摄取的金相图像测量其孔隙率与孔隙分布时，采取图像背底固 定法较好，利用高倍物镜(100 ×，50 ×)摄取的金相图像测量其孔隙率与孔隙分布时，采取峰值法较好；测量视场 数由孔隙测量波动程度与要求达到的测量精度所决定，当测量精度要求达到 3%，置信度为 95%时，需测量的视 场数为 300~330 个。 关键词：陶瓷UO2 ；孔隙率；孔隙分布；定量测量 中图分类号：TF125.42 文献标识码：A 文章编号：1672-7207(2007)03−0409−05 Quantitative measurement of ceramic uranium dioxide porosity and pore distribution HUANG Zhi-feng, CHU Sheng-lin, LIAO Ji-qiao, PU Jian-qiang, ZHEN Ling-zhi (State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China ) Abstract: The method of quantitative measurement of ceramic uranium dioxide porosity and pore distribution was discussed. The results show that the measured value of porosity and pore distribution with four object lens(100 ×, 50 ×, 20 ×, 5 ×) is more accurate and the curve is more smooth than those with single object lens(20 ×). The method of image background grey value is better than the peaking value method for the metallograph grabbed by the low power lens(20 ×, 10×, 5 ×). The peaking value method is better than the method of image background grey value for the metallograph grabbed by the high power lens(100 ×, 50 ×). The number of measured field depends on the fluctuation of porosity measurement and the measured precision. When the con