钛酸锶钡纳米颗粒的粒径调控和分散性改善研究.pdfVIP

Material Sciences 材料科学, 2017, 7(3), 395-402 Published Online May 2017 in Hans. /journal/ms /10.12677/ms.2017.73053 Grain Size Regulation and Dispersion Improvement of Barium Strontium Tiatanate Nanaopowder Mengjie Deng, Xiaohong Xia* School of Materials Science and Engineering, Hubei University, Wuhan Hubei th th th Received: May 11 , 2017; accepted: May 24 , 2017; published: May 27 , 2017 Abstract Barium strontium titanate nanopowder was synthesized by hydrothermal method. The function of dispersant on the particle size regulation and the improvement of powder agglomeration were studied. Effect of annealing on the dispersion of the nanopowder was also investigated. The results turned out that the addition of oleic acid could effectively decrease the particle size of Barium strontium titanate powder, and the smallest particle size could be achieved with the addition of 0.5 ml oleic acid which is about 15 - 25 nm. The dispersibility of the powder was obviously im- proved by post annealing of the hydrothermal synthesized powder, while the particle size was kept unchanged. Keywords Barium Strontium Titanate, Oleic Acid, Particle Size, Dispersibility 钛酸锶钡纳米颗粒的粒径调控和分散性 改善研究 邓梦杰，夏晓红* 湖北大学材料科学与工程学院，湖北 武汉 收稿日期：2017年5月11 日；录用日期：2017年5月24 日；发布日期：2017年5月27 日 *通讯作者。 文章引用: 邓梦杰, 夏晓红. 钛酸锶钡纳米颗粒的粒径调控和分散性改善研究[J]. 材料科学, 2017, 7(3): 395-402. /10.12677/ms.2017.73053 邓梦杰，夏晓红 摘 要 本文用水热法制备了钛酸锶钡纳米颗粒，研究了分散剂的添加对粉末粒径的调控及分散性能的影响，分 析了退火处理对最终产物分散性能的影响。研究表明：通过添加油酸为分散剂能有效减小钛酸锶钡粉末 的晶粒尺寸，当油酸量为0.5 ml时，粉末粒径最小，大约15~25 nm 。退火处理后，钛酸锶钡纳米颗粒的 分散性得到明显改善。 关键词