光谱匹配技术用于磺胺类抗生素HPLC检测的研讨.pdfVIP

光谱匹配技术用于磺胺类抗生素HPLC检测的研究 魏新军颜振敏南海娟张永生王伟华 (河南科技学院食品学院．湃离耱乡453003) 熵要：究了z扳橱障硎离教液翱色^I辫攸榆渊磺眩攫摅嫩索的成分议荆技术，利蠲二极镑|垮矧获取的光谗圈辩峰∞ 纯度进豁手1j毛蛙剥和仪器自动躁配。簌优化的色谗条件下，磺胺嘭疑、磷微掣黎孵碇、磺胺”一：甲髓犍、磺胺甲蒸 鼯啜II!璧、礴弑二二甲镊嘹虢和磺敝睡嚼啉分离良始．利用峰的醐、巾、矫部悲满的一致牲确认峰的缝度。通过玛标 准光谱豫瘁的踬配，张像舒时间一一致的赫础l二，对蜜硒；群晶-{j磺酸畿执俸索鳃分．鬟迸-步确认，W以丰棼除甜样晶 的锻阳性刿新。 关键调；食品科学技术虢砌掌瓣；蘸绶液榴色滋：二二搬管降弼；光潜瓤配；磺胺凌抗嫩索 on SuIfaAntibiotics StudyDetecting bySpectralMatching of Performance TechnologyHigh LiquidChromatography WEI Zhenmin，NAN Xinjan，YAN Haijuan，ZHANGYongsheng， WANGⅥbihua ofFood InstituteofScienceand (School Science，Henan ofthediode detectionHPLCsulfaantibiotic componentsrecognition Abstract：Studyarray technology, 3D ofthe and ofthe ofmanual and map peak peakpurlty composition andautomatic inthe nmtchingequipment．Chromatography havebeen goodseparated，the couldbeconfirmedu瓣ofthecoherenceofthe peak peaksbefore．middle。rearspeetrunl, purity making withastandardof retentiontimeonthebasisof of libraryspectral matching，the consensus．Samples sulfilantibiotic confirmedthatIhe canbeexcludedfromthefalse components-further samples positive judgment． science basic Keywords：foodtechnologysubject，HP∽，photodiodearray·spectralmatching，sulfa antibiotics 动物源蚀食黼中磺姣类药物檎溯常嘲的为液栩色j!{!}法。目J；iii，灏肉像柯不少关下动物潦性☆晶tj}】磺胶燮 药物的液捆色谱捡测方法报