双相高强度管线钢组织性能与工艺控制.docVIP

双相高强度管线钢组织性能与工艺控制 周 民，杜林秀，衣海龙，刘相华 （东北大学轧制技术及连轧自动化国家重点实验室 辽宁 沈阳110004） 摘要：根据管线钢要求中高强度及高韧性的特点，基于超低碳微合金思路Controlling on Microstructure and Process of Dual Phase Pipeline Steel with High Strength ZHOU Min DU Lin-xiu YI Hai-long LIU Xiang-hua (State Key Lab of Rolling Technology and Automation, Northeastern University, Shenyang Liaoning 110004 China) Abstract: According to the property of high strength and high Toughness for high grade pipeline steels, alloy design as ultralow-Carbon microalloyed. For X100 pipeline steel, cooling with three stages was applied after controlled rolling, during these stages, dislocation recovery, sub-grains, deformation-induced precipitation, acicular ferrite and lathe bainite formed, also precipitations grew and carbide accumulated. Fine grain strengthening, sub-structure strengthening and dispersion strengthening was promoted. Cooling mechanism and microstructure transformation in different stages was described. Dual-phases microstructure, bainite, M/A islands, twin transformation mechanism were discussed. The results of mechanical properties indicate that, yield-to-strength ratio is low, yield point is unconspicuous, strength and Toughness is in high level. Key words: M/A islands, fine twin, bainite, cooling with three stages, dislocation wall 前 言 石油、天然气的长距离运输需要高强度、高韧性的管线钢，尤其是位于西欧、北美、北极地区的气候恶劣的环境下的石油输送问题[1~3]，研究的重点在于X80、X100甚至X120等级的高钢级管线钢，所有这些材料要求强度与韧性的结合，对于裂纹的止裂性能和塑性变形行为，尤其是裂纹的萌生及扩展都有较高的要求。高钢级管线钢的生产一般情况下可以采用控轧控冷工艺，也可以采用轧制后淬火加回火，作者在实验室采用轧制结束后不同阶段水冷制度得到具有针状铁素体以及板条状贝氏体的双相高强度X100级别的管线钢。 1.实验材料和方法 合金设计基于超低碳微合金思路，采用高Mn，Mo-Nb微合金化，其实验钢的化学成分为（wt%）：0.06C，0.23Si，1.9Mn，0.005P，0.003S，0.052Nb，0.008Ti，0.28Mo，0.25Ni，0.23Cr，0.20Cu，0.025Al采用150kg真空冶炼炉冶炼，而后将其锻成120mm120mm×l的坯料，轧制及控制冷却试验在东北大学轧制技术及连轧自动化国家重点实验室φ450轧机上进行，轧制完成后得到12mm厚的材料，控制冷却采用三阶段冷却：首先轧制结束后在空气中冷却60s，而后以20~30℃/s的冷却速度快速冷却10~15s，最后空冷至室温。实验材料的拉伸试样采用圆棒状拉伸试样，拉伸实验在WAW-100型微机控制电液伺服万能试验机上进行，拉伸的速度为5mm/min。冲击试样纵向取样，冲击试验在9250 Instron9250HV型落锤冲击试验机上进行，测定室温、-20℃时的冲击值，并利用SEM观察试样的断口形貌。金相试样显微组织观察在LEICA DMIR