原创力文档Development of an ultra high performance liquid chromatography tandem mass spectrometry method for high throughput determination of organophosphorus flame retardants in environmental water英文文献.pdfVIP
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Journal of Chromatography A, 1218 (2011) 6705–6711
Contents lists available at ScienceDirect
Journal of Chromatography A
j o u r n a l h o m e p ag e: w w w. elsev /locat e / c h roma
Development of an ultra-high-performance liquid chromatography–tandem
mass spectrometry method for high throughput determination of
organophosphorus flame retardants in environmental water
Xiao-wei Wang, Jing-fu Liu ∗ , Yong-guang Yin
State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Centerfor Eco-Environmental Sciences, Chinese Academy of Sciences,
P.O. Box 2871, Beijing 100085, China
a r t i c l e i n f o a b s t r a c t
Article history: Widely used as flame retardants, organophosphate esters (OPEs) are now broadly present in the indoor
Received 30 May 2011 and outdoor environments. Currently available liquid chromatography–tandem mass spectrometry
Received in revised form 11 July 2011 (LC–MS/MS) methods share some drawbacks with gas chromatography (GC) methods, including time
Accepted 13 July 2011
consuming, limited target OPEs, incomplete separation capability for some OPEs and low throughput. In
Available online 25 July 2011
this study, a fast and high throughput LC–MS/MS method was developed. For the first time, all the twelve
OPEs that have been studied in literature, ranging from the very polar and volatile trimethyl phosphate
Keywords:
to the very hydrophobic an
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