美国环保局 EPA 试验 方法 3500b.pdf

METHOD 3500B ORGANIC EXTRACTION AND SAMPLE PREPARATION 1.0 SCOPE AND APPLICATION 1.1 Method 3500 provides general guidance on the selection of methods used in the quantitative extraction (or dilution) of samples for analysis by one of the semivolatile or nonvolatile determinative methods. Cleanup and/or analysis of the resultant extracts are described in Chapter Two as well as in Method 3600 (Cleanup) and Method 8000 (Analysis). 1.2 The following table lists the extraction methods, the matrix and the analyte category. SAMPLE EXTRACTION METHODS FOR SEMIVOLATILES AND NONVOLATILES Method # Matrix Extraction Type Analytes 3510 Aqueous Separatory Funnel Semivolatile Nonvolatile Liquid-Liquid Extraction Organics 3520 Aqueous Continuous Liquid- Semivolatile Nonvolatile Liquid Extraction Organics 3535 Aqueous Solid-Phase Extraction Semivolatile Nonvolatile (SPE) Organics 3540 Solids Soxhlet Extraction Semivolatile Nonvolatile Organics 3541 Solids Automated Soxhlet Semivolatiles Nonvolatile Extraction Organics 3542 Air Sampling Train Separatory Funnel Semivolatile Organics Soxhlet Extraction 3545 Solids Pressurized Fluid Semivolatile Nonvolatile