不同产地砂仁的挥发油GC.docVIP

不同砂仁GC-MS及重金属残留测定综合评价 成都中医药大学，四川 成都611137；教育部中药材标准化重点实验室，中药资源系统研究与开发利用省部共建国家重点实验室培育基地 摘要:目的 对5个产地砂仁的挥发油成分及重金属元素进行测定，结合灰色关联分析法从其主要有效成分和重金属残留两个检查测指标对不同产地砂仁的质量进行评价。方法 采用气相色谱和质谱联用技术气相色谱和质谱联用技术 doi：10.3969/j.issn.1003-9783.2016.02 Evaluate the volatile?oil by GC-MS and heavy metals residue in Villosum from different areas AO Hui, LIU Hong-mei, WANG Jiangrui, FANG Chengxin, XU Li,GUO Li, PENG Cheng,YE Qiang* (Chengdu University of Traditional Chinese Medicine. The Ministry of Education Key Laboratory of standardization of Chinese herbal medicine, The Breeding Base of State Key Laboratory of resources systems research and development Utilization of Chinese Herbal Medicines Constructioned by The Ministry of Science and Technology of the PRC and Sichuan Province, Chengdu, 611137, China) Abstract: Objective：To determine the volatile oil and heavy metals in Amomum villosum from different parts, and combine the gray relational analysis to investigate the main effective components and heavy metal residues to evaluate the quality of different origin of Amomum villosum.Provide an evidence for?evaluating Amomum villosum medicinal materials quality and the clinical medication safety. Methods：Combining the GS - MS technique with mass spectrometry library retrieval system to identfy the structure of Amomum villosum volatile oil components, and applicating the chromatographic peak area normalization method to determine the content of each component; Analysising the lead, chromium, copper contents of Amomum villosum in different regions by microwave digestion and graphite furnace atomic absorption spectrophotometry ，combined with the grey correlation analysis method to analyze the all datas. Results：Bornyl acetate content in five different origin of Amomum villosum is the highest in all, camphor next, Amomum villosum from YangChun area is the highest content of bornyl acetate; lead’s content ranges between 0.6400 μg.g-1 and 0.8803μg.g-1, chromium’s content ranges between 0.7463 μg.g-1 a