2.氘在氧化钨中的滞留.pptVIP

Deuterium retention in tungsten oxide under low energy plasma exposure Abstract They have studied deuterium (D) retention in tungsten oxide (WO3) films and thermal release of deuterium D-retention in W has been studied for comparison They find that D-uptake in WO3 film is much larger than in W. According to thermal desorption, release of D2 occurs at 180 and 450 C 1.Introduction Oxide layers exist naturally on metal surfaces and will be formed due to gas introduction for tritium removal Thus, deuterium retention in oxide layers and thermal release of deuterium are important for designing nuclear fusion devices The amount of D retained in the films were analyzed by detecting particles from the nuclear reaction (NRA), using 0.7 MeV ions Dependence of D retention in films on V and D2 gas pressure is described and this is compared with D retention in W and in WO3 under DC discharge. Thermal release of D2 is also presented 2. Experimental procedures films were prepared by oxidation of tungsten metal sheet(99.95% purity) of 0.2 mm in thickness in air at 550 C for 1 h Crystalline structure of the film is examined by X ray-diffraction (XRD) and ascribed to orthorhombic or monoclinic structure Rutherford backscattering spectroscopy (RBS) of 1.8 MeV He+ and 2 MeV H+ were used to obtain the film thickness and composition The amount of D retained in the films were analyzed by detecting a particles from the nuclear reaction, D( , )p, using 0.7 MeV ions 3. Results and discussion D-uptake in increases with increasing V, while D-uptake in W saturates at 1.5 kV. It is noticed that D-uptake in is much larger than in W. D-uptake takes its maximum at 0.5 Torr for both and W D-uptake saturates at 10 min and less than 5 min for and W, respectively From the results of D-retention for DC-plasma exposure shown in Fig. 4, where D-retention monotonically increases with D ion energy, the effective energy of D at V = 1.5 kV is estimated to 100 eV