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耐火材料的微观结构外文文献.pdf

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Available online at ScienceDirect Journal of the European Ceramic Society 35 (2015) 1955–1970 Inﬂuence of microstructural characteristics on fracture toughness of refractory materials Ana García-Prieto a , Manuel Dos Ramos-Lotito a,b , Delia Gutiérrez-Campos b , Pilar Pena a , Carmen Baudín a,∗ a Instituto de Cerámica y Vidrio, CSIC, Kelsen 5, Madrid 28049, Spain b Universidad Simón Bolívar, Dept. Ciencia de los Materiales, Valle de Sartenejas, Caracas 1080, Venezuela Received 28 July 2014; received in revised form 15 December 2014; accepted 16 December 2014 Available online 13 January 2015 Abstract Basic relationships between the microstructure and the texture of refractories and their toughness have been established. A series of commercial materials has been chosen in order to highlight the inﬂuence of microstructural characteristics on fracture behaviour and associated toughness. Silica, silica–alumina and silica–alumina–zirconia based shaped refractories and a calcium aluminate cement bonded concrete have been analysed. Extensive microstructural characterisation has been performed using a combination of techniques, including chemical analysis by X-ray ﬂuores- cence, X-ray diffraction, reﬂected light optical microscopy and scanning electron microscopy with analysis by dispersive energies. Fracture has been characterised using stable fracture tests of SENB tested in 3 point bending. Stability was reached in displacement and crack mouth opening displacement controlled tests. Size effect has be