年产15万吨合成氨脱碳工段初步工艺毕业设计论文121.docVIP

摘 要 本设计是年产十五万吨合成氨脱碳工段的初步工艺设计。本文从多种合成氨脱碳方法的利弊考虑，最终选择本菲儿热钾碱法和两段吸收两段再生的工艺流程，达到最终脱去合成气中的二氧化碳和吸收液的再生。脱碳工段是合成氨工程中必不可少的工段之一，因为如果这些二氧化碳不在合成氨工序前及时除净，氨的合成就会受到影响；同时二氧化碳本身是制取尿素、化肥等产品的原料，也可加工成干冰、食品级二氧化碳，并且二氧化碳是氨合成催化剂的毒物，因此必须除去它。其中二氧化碳吸收塔和溶液再生塔是脱碳过程中不可缺少的塔设备。设计内容主要包括生产工艺的确定和比较、物料衡算和能量衡算、设备的选型与设计和管道尺寸设计。附带的图纸有带控制工艺流程图和二氧化碳吸收塔设备结构图。 关键词：热钾碱法； 脱碳； 工艺设计 Abstract This design is the annual output of one hundred and fifty thousand tons of synthetic ammonia decarbonization section preliminary process design. From considering the pros and cons of a variety of synthetic ammonia decarbonization method, this paper finally choose this Benfica hot alkaline potassium and two regeneration absorb two paragraphs to remove carbon dioxide from the syngas and eventually achieve the regeneration of the solution. Decarbonization section is one of the indispensable section in synthetic ammonia, Because if the carbon dioxide is not remove out in time in the synthetic ammonia process, ammonia synthesis will be affected;At the same time itself is a raw material for preparing urea, fertilizer and other products ,it can also be processed into dry ice, food grade carbon dioxide, and carbon dioxide is the poison of ammonia synthesis catalyst, so you must remove it. carbon dioxide absorption tower and solution regeneration tower is indispensable in the process of decarbonization tower equipment. Finally the design content mainly includes the determination and comparison of production process, material balance and energy balance calculations, the selection and design of the equipment and the design of pipe size. Besides these, it includes the drawing of controllable technological process, the equipment structure drawing of the absorbing tower . Keywords: Hot alkaline potassium; Decarburization; Process design  目录  TOC \o 1-3 \h \z \u  HYPERLINK \l _Toc390080570 1 合成氨脱碳工艺概述  PAGEREF _Toc390080570 \h 5  HYPERLINK \l _Toc390080571 1.1合成氨脱碳方法及工艺的选择  PAGEREF _Toc390080571 \h 5  HYPERLINK \l _To