超临界流体色谱提纯z-藁本内酯-化学工艺专业论文 word格式.docxVIP

目录第一章文献综述 ....................................................................................................... 11.1 超临界流体色谱..............................................................................................1SFC 分离原理1SFC 流动相2SFC 固定相3SFC 制备装置51.2 SFC 制备技术应用51.3 超临界流体中扩散系数测定..........................................................................71.3.1 似稳态法................................................................................................81.3.2 毛细管法................................................................................................81.3.3 非稳态测定法........................................................................................81.4 超临界流体中吸附平衡研究..........................................................................91.4.1 静态法....................................................................................................91.4.2 动态法....................................................................................................91.4.3 超临界流体中吸附平衡模型.............................................................. 111.5 Z-藁本内酯 111.5.1 Z-藁本内酯结构及性质 111.5.2 Z-藁本内酯分离提纯技术 121.6 研究内容与意义............................................................................................13第二章SFC 提纯 Z-藁本内酯工艺研究152.1 实验方法........................................................................................................162.1.1 实验原料与试剂..................................................................................162.1.2 实验装置..............................................................................................172.1.3 实验步骤..............................................................................................172.2 Z-藁本内酯分析方法182.2.1 分析条件..............................................................................................192.2.2 Z-藁本内酯标准曲线192.2.3 分析步骤..............................................................................................202.3 结果与讨论......................................................