非晶陶瓷中温塑性形变的实现与机理研究-材料科学与工程;材料学专业论文 word格式.docx

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非晶陶瓷中温塑性形变的实现与机理研究-材料科学与工程;材料学专业论文 word格式.docx

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非晶陶瓷中温塑性形变的实现与机理研究-材料科学与工程;材料学专业论文 word格式

ABSTRACTCeramicsareknowntobehardandbrittle.Theynormallyexhibitlittletonoplasticdeformationpriortofracture.Thisisaconsequenceofthestrongionicandcovalentbonds,whichmakethemovementofdislocation through thestructuredifficult.Inrecentyears,someresearcherstriedtoimprovetheplasticitybydevelopingamorphousceramics.Becauseofthelong-distancedisorderingstructure,thereexistsnonedislocationandgrainboudaryintheamorphousmaterials,whichavoidsthestructurallimitsofthecrystallineceramics.Inthispaper,weinvestigatedthemoderatetemperaturecompressivebehavioroftheAl2O3-ZrO2,Al2O3-SiO2andAl2O3-MgOamorphousceramcis.Effectsofthetemperatureandcrystallitesonthecompressivebehaviorwerealsoaddressed.Theprepatationofamorphoussampleincludedtheproductionofamorphous powdersandthehotpressingofthecyclinders.Amorphouspowderswereobtainedthroughthecalcinationofthepercursor.Thecylinderswerehotpressedbyusingacubichydraulicpressingmachine.Amorphoussamples wereallfracturedintheelasticdeformationregionwhencompressedatroomtemperature.Thelargestcompressivestrainwassmallerthan10%.Thecompressivestrainsatroomtemperaturewereacributedtothecompressionofthepossibleporesandtheformationofshearbandsintheamorphousmatrix.WhentheamorphousAl2O3-ZrO2sampleswerecompressedat500-700°C,thebrittlefracturetransitedtoplastic deformationwiththeincreasingtemperature.Thesamplecompressedat700°Cexhibitedelasticityuptoastrain of28%followedbyaplateauregiontoabout35%.Theelasticmoduluswas2870MPa.Theexistenceofnanocrystalsintheamorphoussampleswasfoundtoleadtoanincreaseofthecompressiveporperty.However,excessnanocrystalswouldinducethenegativeeffectonthecompressivebehavior.Whencompressedat600-800°C,theamorphousAl2O3-SiO2exhibitedhighelasticity.Thesampleswerestillintheelasticregionbeforeunloading.Theelasticmodulusreducedwiththeincreasingtemperature.Theelasticmoduluswas1922MPawhenthe sample was compressedat800°C.Amorphous Al2O3-MgO samples werefacturedintheelasticregionwhencompressedat500-600°C.Duringthecompressiontestoftheamorphousceramics,theporesw