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多晶X射线衍射仪技术基础-微构分析测试中心
X
微构分析实验室 多晶 射线衍射仪实验技术手册
多晶X 射线衍射仪
实验技术基础
布 莱 格 科 技 ( 北 京 ) 有 限 责 任 公 司
I
· ·
X
微构分析实验室 多晶 射线衍射仪实验技术手册
目 录
前 言·································································································· 1
第一章 X射线基础·················································································· 3
1.1 概述····························································································· 3
1.2 X 射线的产生················································································· 5
1.3 X 射线管工作条件的确定·································································· 6
1.4 X 射线光谱···················································································· 8
1.4.1 连续光谱·············································································· 8
1.4.2 特征光谱·············································································· 9
1.5 物质对X 射线的吸收,实验波长及滤波片的选择··································11
1.5.1 线吸收系数··········································································11
1.5.2 质量吸收系数·······································································11
1.5.3 吸收系数与波长及元素的关系················································· 12
1.5.4 实验波长的选择··································································· 12
1.5.5 滤波片················································································13
1.6 晶体对X 射线的衍射······································································ 13
1.6.1 衍射方向·····························
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