纳米二硫化钼的形态可控合成及其催化与润滑性能研究-环保装备及环境监测工程专业论文.docx

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纳米二硫化钼的形态可控合成及其催化与润滑性能研究-环保装备及环境监测工程专业论文.docx

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纳米二硫化钼的形态可控合成及其催化与润滑性能研究-环保装备及环境监测工程专业论文

wasalsotheactivesiteincaseofthecatalyticdegradationofmethylorange.ThoughtheBETsurfaceoftheMoS2nano-ballswasobviouslylowerthanthatofthenano-slices,theyhadacatalyticactivityclosetothenano-slicesbecauseoftheirlargerabsorbanceinvisiblelightregion. ThecatalyticdegradationofmethylorangecouldbeimprovedbytheincreasedMoS2content,acid solutionandthelowconcentrationofmethylorange.MoS2nano-slicesnotonlyhadhighcatalyticactivity,butalsocouldberegeneratedconveniently.ThecatalysisofMoS2formethylorangedegradationdidnotneedspecialultravioletlights,andespeciallytheMoS2catalystscouldbeused for manytimes.Thus,theMoS2catalystshadsomepotentialindustrialapplicationvalues.Subsequently,thepreparationandthecatalyticpropertiesofnano-MoS2/TiO2compositeswerestudied.TheresultsshowedthatMoS3/TiO2couldbepreparedviathedepositionofMoS3onthesurfaceofnano-TiO2.TheMoS3/TiO2compositeswould bechanged intonano-MoS2/TiO2catalysts aftercalcinationandactivation.Thenano-MoS2/TiO2compositecatalystswereofhigh-activitycatalysisforthedegradationofmethylorangeandhadpotentialapplicationinwastewatertreatment.Nano-MoS2wastheactivecatalystcomponentinthenano-MoS2/TiO2composite.ThecompositecatalysthadhigheractivitythanTiO2andpurenano-MoS2.TiO2functionedasbothasupportandacocatalyst.MoS2onthesurfaceofthecompositecatalystwascomposedof nano-sliceswith10?30nmlengthand~8nmthickness.Oneofnano-MoS2 edgesurfaceslinked withthematrix,and otherswereexposedto the environment.Thus,the compositecatalyst hasvery highBETsurfaceandexcellentcatalyticactivities.Moreover,theintercalationbehaviorofMoS2withdifferentmorphologieswasstudiedbytheexfoliatingandrestackingmethod.TheresultsshowedthattheMoS2sliceshadthehighestintercalationactivitywhiletheMoS2nano-ballsthelowestone.Theexfoliatingandrestacking behaviorsoftheMoS2 slicesweredifferentwiththoseofthebulkMoS2platelets.Therestackedproductsfromthenano-MoS2monolayersuspensionpresentedsimilarcharacteristicswiththeexfoliatednano-MoS2.Thisindicatedthatnano-MoS2monolayersdidnotrestackregularlyalongca