基于zr-mof的不同形态介孔zro2的制备及表征-preparation and characterization of different mesoporous z ro2 based on zr - mof.docxVIP

3.3.3样品UiO-67的热重（TG）分析223.3.4样品UiO-67的透射电子显微镜（TEM）分析233.3.5样品UiO-67的氮气吸附和孔径分析243.4 小结...................................................................................................................................25第四章热分解金属有机框架材料UiO-66 制备介孔ZrO2/C和ZrO2274.1引言..................................................................................................................................274.2实验部分..........................................................................................................................274.3 材料的表征方法及条件..................................................................................................284.3.1样品ZrO2/C和ZrO2的X射线粉末衍射表征284.3.2样品ZrO2/C透射电子显微镜（TEM）分析29样品ZrO2/C-flowN2的热重（TG）表征31样品ZrO2/C-flowN2、ZrO2/C-noflowN2的氮气吸附和孔径分析324.3.5不同条件下制备的氧化锆的氮气吸附和孔径分析..............................................................324.4小结..................................................................................................................................34 第五章介孔ZrO2/C 对刚果红溶液的吸附...............................................................35 5.1 引言...................................................................................................................................355.2刚果红标准曲线的绘制................................................................................................355.3刚果红溶液吸附试验....................................................................................................365.3.1不同质量的样品ZrO2/C对刚果红溶液的吸附性能365.3.2不同时间内样品ZrO2/C对刚果红溶液的吸附效率375.4 结果与讨论.......................................................................................................................375.4.1不同质量的样品ZrO2/C对刚果红溶液的吸附性能375.4.2不同时间内样品ZrO2/C对刚果红溶液的吸附效率395.5 小结...................................................................................................................................40第六章金属有机框架材料UiO-67 孔道中灌入咪唑并对质子导电性的研究416.1 引言......................................................................................................................