赪桐、翻白叶树的质量标准分析-analysis of quality standards of paulownia fortunei and aesculus chinensis.docx

1实验材料.................................................................................................591.1药材......................................................................................................591.2仪器......................................................................................................591.3试剂.......................................................................................................592实验方法与结果......................................................................................602.1翻白叶树药材化学成分预试...............................................................602.2翻白叶树药材中原儿茶酸的含量测定................................................643小结.........................................................................................................76五翻白叶树药材质量标准的草案.............................................................781翻白叶树质量标准..................................................................................782翻白叶树质量标准注释..........................................................................81第三部分讨论............................................................................................87参考文献.....................................................................................................89综述.....................................................................................................92致谢...................................................................................................101攻读学位期间发表的学术论文目录.........................................................102广西中医药大学研究生学位论文作者声明.............................................104个人简历...................................................................................................105附：科技查新报告中文摘要目的：对赪桐和翻白叶树进行真伪、优劣评价，并初步建立赪桐和翻白叶树的质量标准。方法：分别对赪桐和翻白叶树通过原植物鉴别、性状鉴别、显微鉴别与理化鉴别的方法进行生药学鉴别研究，按《中国药典》2010年版的方法进行药材水分、灰分、浸出物等限量研究；此外，采用HPLC，以原儿茶酸为对照品，对翻白叶树进行含量测定。结果：①原植物形态、性状特征、显微特征与薄层色谱对赪桐和翻白叶树均具有鉴别意义。②赪桐药材水分含量不得超过10.0%；总灰分含量不得超过11.0%；酸不溶性灰分含量不得超过0.55%；醇溶性浸出物含量不得低于14.0%。③翻白叶树药材水分含量不得超过14